The solubilities of bis(benzoxazolyl-2-methyl) sulfide in ethanol, 1-butanol, 2-propanol, chlorobenzene, toluene, o-xylene, and ethanol + water were measured by a synthetic method. The laser monitoring observation technique was used to determine the disappearance of the solid phase in the solid + liquid mixture. All data were measured in the temperature range from (273.25 to 325.25) K at atmosphere pressure. The effect of solvent composition and temperature on the solubility was discussed. For all solvents studied, the data are well fitted with a semiempirical Apelblat equation.