The solubility of 2-chloro-4,6-dinitroresorcinol in ethanol at (299.35 to 343.75) K, methanol at (299.75 to 333.35) K, acetic acid at (299.35 to 343.15) K, ethyl acetate at (298.75 to 344.95) K, and water at (298.85 to 341.95) K was measured using the ultraviolet absorption method. The 2-chloro-4,6-dinitroresorcinol solubility in each solvent increases with increasing temperature. Results of these measurements were correlated with a semiempirical equation. For the systems studied, the semiempirical equation was found to provide reasonable mathematical representation, and the three parameters of the semiempirical equation were obtained.