Journal of Industrial and Engineering Chemistry, Vol.20, No.1, 245-258, January, 2014
A comparative study of hydroxyapatite nanostructures produced under different milling conditions and thermal treatment of bovine bone
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In the present investigation the effects of milling parameters (time, atmosphere, and media) and
chemical composition of raw materials on the mechanochemical synthesis of nanocrystalline
hydroxyapatite (n-HAp) were studied. For a comparative study of the mechanically activated samples versus thermally treated specimen (natural origin), n-HAp was also produced via annealing of bovine bone at 800 ℃ for 2 h. The gained powders exhibited average sizes about 32 and 27 nm under air atmosphere, and about 32 and 34 nm under argon atmosphere. TEM images confirmed the formation of n-HAp with various morphologies under different experimental conditions.
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