Study on α-alumina precursors prepared using different ammonium salt precipitants

Du-Chul Shin; Seong Soo Park; Joo Hyun Kim; Seong Soo Hong; Jong Myung Park; Seung Ho Lee; Dae Sung Kim; Gun Dae Lee

Journal of Industrial and Engineering Chemistry, Vol.20, No.4, 1269-1275, July, 2014

DOI10.1016/j.jiec.2013.07.003 Export Citation

Study on α-alumina precursors prepared using different ammonium salt precipitants

Du-Chul Shin, Seong Soo Park, Joo Hyun Kim¹, Seong Soo Hong², Jong Myung Park³, Seung Ho Lee⁴, Dae Sung Kim⁴, and Gun Dae Lee^†

Department of Industrial Chemistry, Pukyong National University, Busan 608-739, Republic of Korea
¹Department of Polymer Engineering, Pukyong National University, Busan 608-739, Republic of Korea
²Department of Chemical Engineering, Pukyong National University, Busan 608-739, Republic of Korea
³Graduate Institute of Ferrous Technology, Pohang University of Science and Technology, Pohang 790-784, Republic of Korea
⁴Eco Composite Materials Center, Korea Institute of Ceramic Engineering & Technology, Seoul 153-801, Republic of Korea

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Nano-sized α-Al2O3 platelets have been produced by the precipitation method employing the starting material of Al(NO3)3·9H2O and ammonium salt precipitants, such as the NH4OH, (NH4)2CO3 and NH4HCO3. The effects of chemical composition of ammonium salt precipitants and aging time of precipitated product on the formation of precursor and final product of α-Al2O3 particles were studied. The precursors with different crystal structures were formed depending on the chemical composition of precipitant and the agglomeration of final α-Al2O3 particles was found to be greatly affected by the precipitant. The aging time of precipitated precursor also influenced the agglomeration of final aalumina particles.

Keywords:α-Alumina nanoparticle;Precursor;Precipitant;Aging time;Agglomeration

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Okada K, Nagashima T, Kameshima Y, Yasumori A, Tsukada T, J. Colloid Interface Sci., 253(2), 308 (2002)
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Du XL, Wang YQ, Su XH, Li JG, Powder Technol., 192(1), 40 (2009)
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Zhu ZF, Sun HJ, Liu H, Yang D, J. Mater. Sci., 45(1), 46 (2010)
Li JG, Sun X, Acta Mater., 48, 3103 (2000)
Daimon K, Kato E, J. Cryst. Growth, 75, 348 (1986)
Stoica G, Perez-Ramirez J, Chem. Mater., 19, 4783 (2007)
Xiao J, Deng H, Wan Y, Li J, Liu Y, J. Central South University of Technol., 13, 367 (2006)
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[2] Wu Y, Zhang Y, Pezzotti G, Guo J, Mater. Lett., 52, 366 (2002)

[3] Mazloumi M, Khalifehzadeh R, Sadrnezhaad SK, Arami H, J. Am. Ceram. Soc., 89(12), 3654 (2006)

[4] Lu H, Sun H, Mao A, Yang H, Wang H, Hu X, Mater. Sci. Eng. A-Struct. Mater. Prop. Microstruct. Process., 406, 19 (2005)

[5] Wu YQ, Zhang YF, Huang XX, Guo JK, Ceram. Int., 27, 265 (2001)

[6] Lu HX, Sun HW, Li GX, Chen CP, Yang DL, Hu X, Ceram. Int., 31, 105 (2005)

[7] Parida KM, Pradhan AC, Das J, Sahu N, Mater. Chem. Phys., 113(1), 244 (2009)

[8] Wang S, Li X, Wang S, Li Y, Zhai Y, Mater. Lett., 62, 3552 (2008)

[9] Zeng M, Ma Y, Wang Y, Pei C, Ceram. Int., 38, 6951 (2012)

[10] Wen HL, Chen YY, Yen FS, Huang CY, Nanostruct. Mater., 11, 89 (1999)

[11] Jeong JY, Park SW, Moon DK, Kim WJ, J. Ind. Eng. Chem., 16(2), 243 (2010)

[12] Okada K, Nagashima T, Kameshima Y, Yasumori A, Tsukada T, J. Colloid Interface Sci., 253(2), 308 (2002)

[13] Li JG, Ikegami T, Lee JH, Mori T, Yajima Y, J. European Ceram. Soc., 20, 2395 (2000)

[14] Su-peng, Guo-xueyi, Ji-shujun, Adv. Powder Technol., 20(6), 542 (2009)

[15] Sun XD, Li JG, Zhang F, Qin XM, Xiu ZM, Ru HQ, You J, J. Am. Ceram. Soc., 86(8), 1321 (2003)

[16] Wu Z, Shen Y, Dong Y, Jianqing J, J. Alloy. Compd., 467, 600 (2009)

[17] Du XL, Wang YQ, Su XH, Li JG, Powder Technol., 192(1), 40 (2009)

[18] Hayashi K, Toyoda S, Nakashima K, Morinaga K, J. Ceram. Soc. Jpn., 98, 444 (1990)

[19] Zhu ZF, Sun HJ, Liu H, Yang D, J. Mater. Sci., 45(1), 46 (2010)

[20] Li JG, Sun X, Acta Mater., 48, 3103 (2000)

[21] Daimon K, Kato E, J. Cryst. Growth, 75, 348 (1986)

[22] Stoica G, Perez-Ramirez J, Chem. Mater., 19, 4783 (2007)

[23] Xiao J, Deng H, Wan Y, Li J, Liu Y, J. Central South University of Technol., 13, 367 (2006)

[24] Ma CC, Zhou XX, Xu X, Zhu T, Mater. Chem. Phys., 72(3), 374 (2001)

[25] Kato S, Iga T, J. Chem. Soc. Jpn., 88, 253 (1997)