화학공학소재연구정보센터
Journal of Materials Science, Vol.49, No.13, 4565-4575, 2014
Recrystallization, texture evolution, and magnetostriction behavior of rolled (Fe81Ga19)(98)B-2 sheets during low-to-high temperature heat treatments
In order to study the texture evolution and magnetostriction behavior in the rolled Fe-Ga-B sheets during the heat treatments from low to high temperatures, (Fe81Ga19)(98)B-2 sheets were prepared and investigated. The phase structure, recrystallization, grain size, texture evolution, and magnetostriction behavior during the annealing from 525 to 1200 A degrees C for 1-5 h were investigated using X-ray diffraction, electron backscattering diffraction, and standard strain-gauge measurements. Results indicated that the primary recrystallization temperature for 1-h annealing was found as 525-575 A degrees C in (Fe81Ga19)(98)B-2 sheets. Annealing the sample below 575 A degrees C for 1 h, the release of rolling stress and increase of aOE (c) 100 > eta-fiber texture during the primary recrystallization jointly resulted in a rapid improvement in magnetostriction. After annealed between 575 and 1100 A degrees C for 1 h, the grains of the sheets underwent a normal growth, and the three (alpha-, gamma- and eta-fiber) types of textures kept an approximate balance, leading to a plateau of magnetostriction around 75 ppm. When the abnormal grain growth proceeded above 1100 A degrees C for 1 h, the proportion of eta-fiber texture markedly increased, and the magnetostriction was subsequently increased to 97 ppm. For longer annealing durations, the strong ideal cube texture (eta-fiber) was firstly formed and then changed to undesired texture (gamma-fiber), producing a corresponding magnetostriction peak of 136 ppm at 2 h for the annealing at 1200 A degrees C. The clear correlation among heat treatments, recrystallization, texture, and magnetostriction provides an essential understanding for Fe-Ga-B alloy sheets.