The development of a new non-intrusive computerized image analysis and optical observation method for accurately detecting the vapor-liquid interface in stratified two-phase flows is presented. This technique is applied to a round horizontal sight glass tube using a monochromatic laser sheet for observing two-phase flow patterns and for measuring cross-sectional dry angles and void fractions in these types of flow. The cross-sectional image observed externally is distorted by refraction and is thus reconstructed by computer. From this image, the shape of the vapor-liquid interface is detected and the dry angle and void fraction are accurately determinable over a wide range of conditions for a glass tube of 13.6 mm diameter. Results for dry angle are reported here while the test facility and void fraction measurements are presented in Part II. R-22 and R-410A are the test fluids. Dry angles were quite close to values predicted for stratified flow and much larger than comparable values for air-water flows. (C) 2003 Elsevier Ltd. All rights reserved.