Materials Science Forum, Vol.426-4, 1065-1070, 2003
Formation of ultra-fine grained SUS316L steels by ball-milling and their mechanical properties after neutron irradiation
In order to overcome the irradiation embrittlement in austenitic stainless steels, ultra-fine grained SUS316L steels with very fine TiC particles have been developed. The SUS316L-TiC nanocomposite powders having 1.0 to 2.0 mass % TiC were prepared by ball-milling SUS316L-TiC powder mixtures for 125 h in an argon gas atmosphere. The milled powders were consolidated by hot isostatic pressing (HIP) under a pressure of 200 MPa at temperatures between 700 and 1000 degreesC, and the bulk materials with grain sizes between 100 and 400 rim have been produced. The possibility of using fine-grained TiC particles to pin grain boundaries and thereby maintain the ultra-fine grained structures has been discussed. In order to clarify the effects of the neutron irradiation on mechanical properties of the ultra-fine grained SUS316L steels, Vickers microhardness measurements were performed before and after the irradiation of 1.14 x 10(23) n/m(2) and 1.14 x 10(24) n/m(2). The hardness increased with increasing the dose of the irradiation. However, these increasing rates of the ultra-fine grained steels were much smaller than those of the coarse-grained SUS316L steels having grain sizes between 13 and 50mum.
Keywords:irradiation;nuclear reactor materials;titanium carbide-dispersion;ultra-fine grain;SUS316L;powder ball-milling;hot isostatic pressing;vickers microhardness