The structure and phase composition of dispersion-strengthened composite materials based on multicomponent aluminium alloys of the Al-Cu-Mg and Al-Si-Cu-Fe systems at various stages of mechanical alloying were studied by the methods of optical, scanning electron and ion microscopies, electron probe microanalysis and X-ray diffraction analysis. A possibility of the efficient use of commercial scrap of Al alloy chips and initially large strengthening ceramic particles as the base of composite materials was shown, as well as a possibility of synthesis of strengthening particles during the treatment. After mechanical alloying, these materials possessed a homogeneous and disperse structure, high hardness at room and elevated temperatures and a low linear thermal expansion coefficient.