Silicon carbide nanoparticles as an adsorbent for solid phase extraction of lead and determination by flame atomic absorption spectrometry

Nahid Pourreza; Tina Naghdi

Journal of Industrial and Engineering Chemistry, Vol.20, No.5, 3502-3506, September, 2014

DOI10.1016/j.jiec.2013.12.041 Export Citation

Silicon carbide nanoparticles as an adsorbent for solid phase extraction of lead and determination by flame atomic absorption spectrometry

Nahid Pourreza^†, and Tina Naghdi

Department of Chemistry, College of Science, Shahid Chamran University, Ahvaz, Iran

E-mail:

Silicon carbide nanoparticles were applied as a new solid phase adsorbent for preconcentration of lead ions. Pb(II) ions are adsorbed on silicon carbide nanoparticles, eluted with nitric acid and determined by flame atomic absorption spectrometry. The solid phase extraction conditions were optimized. The calibration graph was linear in the range of 2-150 ng mL-1 (r = 0.9995) with a detection limit of 0.4 ng mL-1. The relative standard deviation for eight measurements of 20 ng mL-1 of Pb(II) was 1.3%. The adsorption capacity was 156.2 mg g-1of Pb(II). The method was applied to determination of Pb(II) in different samples.

Keywords:Lead;Silicone carbide nanoparticles;Solid phase extraction;Preconcentration;Flame atomic absorption spectrometry

[References]

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Rosell A, Palet C, Valiente M, Anal. Chim. Acta, 370, 141 (1998)
Xie F, Lin X, Wu X, Xie Z, Talanta, 74, 836 (2008)
Daftsis EJ, Zachariadis GA, Talanta, 71, 722 (2007)
Suleiman JS, Hu B, Huang CZ, Zhang N, J. Hazard. Mater., 157(2-3), 410 (2008)
Bressy FC, Brito GB, Barbosa IS, Teixeira LSG, Korn MGA, Microchem J., 109, 145 (2013)
Matos Reyes MN, Campos RC, Spectroc. Acta Pt. B-Atom. Spectr., 60, 615 (2005)
Oliva A, Molinari A, Zuniga F, Ponce P, Mikrochim. Acta, 140, 201 (2002)
Soylak M, Aydin A, Food Chem. Toxicol., 49, 1242 (2011)
Soylak M, Onal G, J. Hazard. Mater., 137(2), 1130 (2006)
Wen X, Deng Q, Ji S, Yang S, Peng L, Microchem J., 100, 31 (2012)
El-Shahawi MS, Hamza A, Al-Sibaai AA, Bashammakh AS, Al-Saidi HM, J. Ind. Eng. Chem., 19(2), 529 (2013)
Pourreza N, Fathi MR, Hatami A, Microchem J., 104, 22 (2012)
Baytak S, Kenduzler E, Turker AR, Gok N, J. Hazard. Mater., 153(3), 975 (2008)
Ayata S, Bozkurt SS, Ocakoglu K, Talanta, 84, 212 (2011)
Pourreza N, Fathi MR, Ardan Z, J. Iran. Chem. Soc., 7, 965 (2010)
Al-bishri HM, Abdel-Fattah TM, Mahmoud ME, J. Ind. Eng. Chem., 18(4), 1252 (2012)
Pourreza N, Ghanemi K, J. Hazard. Mater., 178(1-3), 566 (2010)
Parham H, Pourreza N, Rahbar N, J. Hazard. Mater., 163(2-3), 588 (2009)
Tuzen M, Soylak M, Elci L, Anal. Chim. Acta, 548, 101 (2005)
Elci L, Kartal AA, Soylak M, J. Hazard. Mater., 153(1-2), 454 (2008)
Ghaedi M, Mokhtari P, Montazerozohori M, Asghari A, Soylak M, J. Ind. Eng. Chem., http://dx.doi.org/10.1016/j.jiec.2013.05.027 (2013)
Elci L, Soylak M, Uzun A, Buyukpatir E, Dogan M, Fresenius J. Anal. Chem., 368, 358 (2000)
Soylak M, Yilmaz E, J. Hazard. Mater., 182(1-3), 704 (2010)
Pourreza N, Hoveizavi R, Anal. Chim. Acta, 549, 124 (2005)
Barbosa AF, Segatelli MG, Pereira AC, de Santana Santos A, Kubota LT, Luccas PO, Teixeira Tarley CR, Talanta, 71, 1512 (2007)
Ghanemi K, Nikpour Y, Omidvar O, Maryamabadi A, Talanta, 85, 763 (2011)
Pourreza N, Shaikhnajdi K, Talanta, 99, 507 (2012)
Bayazit SS, Inci I, J. Ind. Eng. Chem., 19(6), 2064 (2013)
Ma Q, Cao QE, Zhao Y, Wu S, Hu Z, Xu Q, Food Chem., 71, 123 (2000)
Tan XL, Chang PP, Fan QH, Zhou X, Yu SM, Wu WS, Wang XK, Colloids Surf. A: Physicochem. Eng. Asp., 328, 8 (2008)
Ghassabzadeh H, Mohadespour A, Torab-Mostaedi M, Zaheri P, Maragheh MG, Taheri H, J. Hazard. Mater., 177(1-3), 950 (2010)

[Referenced By]

[1] Zhoua Y, Zanao RA, Barbosa F, Parsons PJ, Krug FJ, Spectroc. Acta Pt. B-Atom. Spectr., 57, 1291 (2002)

[2] Rosell A, Palet C, Valiente M, Anal. Chim. Acta, 370, 141 (1998)

[3] Xie F, Lin X, Wu X, Xie Z, Talanta, 74, 836 (2008)

[4] Daftsis EJ, Zachariadis GA, Talanta, 71, 722 (2007)

[5] Suleiman JS, Hu B, Huang CZ, Zhang N, J. Hazard. Mater., 157(2-3), 410 (2008)

[6] Bressy FC, Brito GB, Barbosa IS, Teixeira LSG, Korn MGA, Microchem J., 109, 145 (2013)

[7] Matos Reyes MN, Campos RC, Spectroc. Acta Pt. B-Atom. Spectr., 60, 615 (2005)

[8] Oliva A, Molinari A, Zuniga F, Ponce P, Mikrochim. Acta, 140, 201 (2002)

[9] Soylak M, Aydin A, Food Chem. Toxicol., 49, 1242 (2011)

[10] Soylak M, Onal G, J. Hazard. Mater., 137(2), 1130 (2006)

[11] Wen X, Deng Q, Ji S, Yang S, Peng L, Microchem J., 100, 31 (2012)

[12] El-Shahawi MS, Hamza A, Al-Sibaai AA, Bashammakh AS, Al-Saidi HM, J. Ind. Eng. Chem., 19(2), 529 (2013)

[13] Pourreza N, Fathi MR, Hatami A, Microchem J., 104, 22 (2012)

[14] Baytak S, Kenduzler E, Turker AR, Gok N, J. Hazard. Mater., 153(3), 975 (2008)

[15] Ayata S, Bozkurt SS, Ocakoglu K, Talanta, 84, 212 (2011)

[16] Pourreza N, Fathi MR, Ardan Z, J. Iran. Chem. Soc., 7, 965 (2010)

[17] Al-bishri HM, Abdel-Fattah TM, Mahmoud ME, J. Ind. Eng. Chem., 18(4), 1252 (2012)

[18] Pourreza N, Ghanemi K, J. Hazard. Mater., 178(1-3), 566 (2010)

[19] Parham H, Pourreza N, Rahbar N, J. Hazard. Mater., 163(2-3), 588 (2009)

[20] Tuzen M, Soylak M, Elci L, Anal. Chim. Acta, 548, 101 (2005)

[21] Elci L, Kartal AA, Soylak M, J. Hazard. Mater., 153(1-2), 454 (2008)

[22] Ghaedi M, Mokhtari P, Montazerozohori M, Asghari A, Soylak M, J. Ind. Eng. Chem., http://dx.doi.org/10.1016/j.jiec.2013.05.027 (2013)

[23] Elci L, Soylak M, Uzun A, Buyukpatir E, Dogan M, Fresenius J. Anal. Chem., 368, 358 (2000)

[24] Soylak M, Yilmaz E, J. Hazard. Mater., 182(1-3), 704 (2010)

[25] Pourreza N, Hoveizavi R, Anal. Chim. Acta, 549, 124 (2005)

[26] Barbosa AF, Segatelli MG, Pereira AC, de Santana Santos A, Kubota LT, Luccas PO, Teixeira Tarley CR, Talanta, 71, 1512 (2007)

[27] Ghanemi K, Nikpour Y, Omidvar O, Maryamabadi A, Talanta, 85, 763 (2011)

[28] Pourreza N, Shaikhnajdi K, Talanta, 99, 507 (2012)

[29] Bayazit SS, Inci I, J. Ind. Eng. Chem., 19(6), 2064 (2013)

[30] Ma Q, Cao QE, Zhao Y, Wu S, Hu Z, Xu Q, Food Chem., 71, 123 (2000)

[31] Tan XL, Chang PP, Fan QH, Zhou X, Yu SM, Wu WS, Wang XK, Colloids Surf. A: Physicochem. Eng. Asp., 328, 8 (2008)

[32] Ghassabzadeh H, Mohadespour A, Torab-Mostaedi M, Zaheri P, Maragheh MG, Taheri H, J. Hazard. Mater., 177(1-3), 950 (2010)