화학공학소재연구정보센터
Journal of Industrial and Engineering Chemistry, Vol.20, No.5, 3815-3820, September, 2014
Performance of hydrate inhibitors in tetrahydrofuran hydrate formation by using measurement of electrical conductivity
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This study tries to investigate the kinetic behavior of THF hydrate formation in the presence of electrolytic inhibitors containing, LiCl, NaCl, KCl, CsCl, MgCl2, CaCl2, and BaCl2·2H2O salts. The experiments were conducted with the initial temperature of 2.3 ℃, and the concentration ranging 1-2% weight of salts. Measurement of electrical conductivity during process was used to study the THF hydrate formation and analyze the inhibition strength of mentioned salts. The results, based on a novel technique, indicate that the inhibition strength depends on the ionic size and electrical charge. The best performance for hydrate inhibition is in the following order: Mg2+ > Li1+ > Ca2+ > Ba2+ > Na1+ > K1+ > Cs1+.
  1. Sloan ED, Koh CA, Clathrate Hydrates of Natural Gases, 3rd ed., CRC Press, Taylor & Francis Group, Boca Raton, 2008.
  2. Ballard AL, Sloan ED, Chem. Eng. Sci., 56(24), 6883 (2001)
  3. Nikbakht F, Izadpanh A, Varaminian F, Mohammadi A, Int. J. Refrig. -Rev. Int. Froid, 35, 1914 (2012)
  4. Sabil KM, Witkamp GJ, Peters CJ, Fluid Phase Equilib., 284(1), 38 (2009)
  5. Wilson PW, Haymet ADJ, Chem. Eng. J., 161(1-2), 146 (2010)
  6. Liu Y, Song Y, Chen Y, Yao L, Li Q, J. Nat. Gas Chem., 19, 224 (2010)
  7. Nagashima K, Yamamoto Y, Takahashi M, Komai T, Fluid Phase Equilib., 214(1), 11 (2003)
  8. Iida T, Mori H, Mochizuki T, Mori YH, Chem. Eng. Sci., 56(16), 4747 (2001)
  9. Bollavaram P, Devarakonda S, Selim MS, Sloan ED, Ann. NY Acad. Sci., 912, 533 (2000)
  10. Devarakond S, Groysman A, Myerson AS, J. Cryst. Growth, 204, 525 (1998)
  11. Conrad V, Tetrahydrofuran Clathrate Hydrate Formation Studied by X-ray Raman Scattering, Faculty of Physics, Technique University Dortmund, 2009.
  12. Kwona YA, Park JM, Jeong KE, Kim CU, Kim TW, Chae HJ, Jeong SY, Yim JH, Park YK, Lee J, J. Ind. Eng. Chem., 17(1), 120 (2011)
  13. Karamoddin M, Varaminian F, Desal. Water Treat., 1 (2013)
  14. Song YC, Yang MJ, Liu Y, Nat. Gas Ind., 28(8), 111 (2008)
  15. Zhou X, Fan S, Liang D, Wang D, Huang N, J. Nat. Gas Chem., 16, 399 (2007)
  16. Maeda K, Katsura Y, Asakuma Y, Fukui K, Chem. Eng. Process., 47(12), 2281 (2008)
  17. Park SS, Kim KJ, J. Ind. Eng. Chem., 19(5), 1668 (2013)
  18. Kashchiev D, Firoozabadi A, J. Cryst. Growth, 241(1-2), 220 (2002)
  19. Alive AM, Yusifov G, Russ. J. Appl. Chem., 81, 588 (2008)
  20. Corak D, Barth T, Hoiland S, Skodvin T, Larsen R, Skjetne T, Desalination, 278(1-3), 268 (2011)
  21. Robert W, Jeffrey A, Desalination Utilizing Clathrate Hydrates, Sandia National Laboratories, 2008.
  22. Lederhos JP, Long JP, Sum A, Christiansen RL, Sloan ED, Chem. Eng. Sci., 51(8), 1221 (1996)
  23. Park KN, Hong SY, Lee JW, Kang KC, Lee YC, Ha MG, Lee JD, Desalination, 274(1-3), 91 (2011)
  24. Marcus Y, Ion Properties, 3rd ed., Marcel Dekker, Inc., New York, 1997.
  25. Kang SP, Chun MK, Lee H, Fluid Phase Equilib., 147(1-2), 229 (1998)
  26. Englezos P, Hall S, Can. J. Chem. Eng., 72(5), 887 (1994)
  27. Dholabhai PD, Parent JS, Bishnoi PR, Ind. Eng. Chem. Res., 35(3), 819 (1996)
  28. Berecz E, Balla-Achs M, Gas Hydrates, Elsevier, Amsterdam, 1983.