화학공학소재연구정보센터
홈 로그인 로그아웃 연락처 사이트맵
Korean Journal of Materials Research, Vol.16, No.3, 198-202, March, 2006
DOI10.3740/MRSK.2006.16.3.198  Export Citation
초음파 화학법에 의한 CdSe 나노 입자의 합성
Sonochemical Synthesis of CdSe Nanoparticles from Mixed Aqueous Solution
성명석, 이윤복1, 김용진2, 김영석3, 김양도†
  • 부산대학교 재료공학부
  • 1부산대학교 유전체 물성연구소
  • 2한국기계연구원 재료기술연구소
  • 3한국생산기술연구원 부산지역본부 차세대생산공정팀
Myoung Seok Sung, Yoon Bok Lee1, Yong-Jin Kim2, Young Seok Kim3, and Yangdo Kim†
  • School of Materials Science and Engineering, Pusan National University, Korea
  • 1Research Center for Deilectric and Advanced Matter Physics, Pusan National University, Korea
  • 2Materials Research Sfation, Korea Institute Of Machiery and Materials, Korea
  • 3Busan Research Center Advanced Manufacturng Technology Team, Korea Institute Of Industial Technology, Korea
E-mail:
Cadmium selenide (CdSe) nanoparticles with the diameter of about 3.4nm have been synthesized from the mixed aqueous solution of distilled water and diethanolamine at room temperature. The cadmium chloride ( [Math Processing Error] ), sodium selenosulfate ( [Math Processing Error] ) were used as the cadmium and selenium source, respectively. The properties of CdSe nanoparticles were characterized by using transmission electron microscopy (TEM), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD) and UV-Vis measurements. CdSe nanoparticles were analyzed to be cubic phase with the absorption excition peaks between 540 and 600 nm. CdSe nanoparticles also showed red-shifted excition peaks with increasing the sonication time. This paper mainly presents the sonication effects on the formation of CdSe nanoparticles prepared from the mixed aqueous solution of distilled water and diethanolamine.
Keywords:cadmium selenide;nanoparticle;sonochemical method
  1. Trindade T, O'Brien P, Pickett NL, Chem. Mater., 13, 3843 (2001)
  2. Peng XG, Manna L, Yang WD, Wickham J, Scher E, Kadavanich A, Alivisatos AP, Nature, 404(6773), 59 (2000)
  3. Gao YM, Wu P, Dwight KM, Wold A, Mater. Res. Bull., 24, 1215 (1989)
  4. Manna L, Scher EC, Alivisatos AP, J. Am. Chem. Soc., 122(51), 12700 (2000)
  5. Peng XG, Adv. Mater., 15(5), 459 (2003)
  6. Peng ZA, Peng XG, J. Am. Chem. Soc., 123(1), 183 (2001)
  7. Suh DJ, Park OO, Jung HT, Kwon MH, Korean J. Chem. Eng., 19(3), 529 (2002)
  8. Zhang X, Xie Y, Xu D, Liu X, Inorg. Chem. Comm., 7, 417 (2004)
  9. Henshaw G, Parkin IP, Shaw G, J. Chem. Soc., Dalton Trans., 231 (1997)
  10. Hyeon TH, Fang MM, Suslick KS, J. Am. Chem. Soc., 118(23), 5492 (1996)
  11. Suslick KS, Science, 247, 1439 (1990)