Korean Journal of Materials Research, Vol.15, No.1, 19-24, January, 2005
초초임계압 발전용 소재의 장시간 열처리에 따른 미세조직 변화와 기계적 특성의 상관관계 연구
A Study on Correlation of Microstructural Degradation and Mechanical Properties of 9-12%Cr-Steel for Ultra-Super Critical Power Generation
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For the good combination of high-temperature strength, toughness and creep property, 9?12% chromium steels are often used for gas turbine compressors, steam turbine rotors, blade and casing. In this study, the correlation of microstructural evolution and mechanical properties was investigated fur the specimens heat-treated at 600, 650 and 700 ? C for 1000, 3000 and 5000 hrs. The microstructure of as-received specimen was tempered martensite with a high dislocation density, small sub-grains and fine secondary phase such as M 2 3C 6 . Aging for long-time at high temperature caused the growth of martensite lath and the decrease of dislocation density resulting in the decrease in strength. However, the evolution of secondary phases had influence on hardness, yield strength and impact property. In the group A specimen aged at 600 ? Cand650 ? C , Laves phase was observed. The Laves phase caused the increase of the hardness and the decrease of the impact property. In addition, the abrupt growth of secondary phases caused decrease of the impact property in both A and B group specimens.
- Kaneko K, Matsumura S, Sadakata A, Fujita K, Moon WJ, Ozaki S, Nishimura N, Tomokiyo Y, Mater. Sci. Eng. A, 374, 82 (2004)
- Klotz UE, Solenthaler C, Ernst P, Uggowitzer OJ, Speidel MO, Mater. Sci. Eng. A, 272, 292 (1999)
- Sklenicka V, Kuchacova K, Svoboda M, Kloc L, Burcik J, Kroupa A, Materials Characterization, 51, 35 (2003)
- Abe F, Horiuchi T, Taneike M, Sawada K, Mater. Sci. Eng. A, 378, 299 (2004)
- Hosoi Y, Wade N, Kunimitsu S, Urita T, J. Nucl. Mater, 461, 141 (1986)
- Miyahara K, Hwang JH, Shimoide Y, Scr. Metall. Mater, 32, 1917 (1995)
- Hald J, Steel Res, 9, 369 (1996)
- Rodak K, Hernas A, Kielbus A, Materials Chemistry and Physics, 9814, 1 (2003)
- Yoshinori M, Kyohei T, Misaki K, Masahiko M, Ryokichi H, Kazuhiro M, Tsukasa A, Toru I, Tetsu-to-Hagane, 88(4), 214 (2002)
- Dimmler G, Weinert P, Kozeschnik E, Cerjak H, Materials Characterization, 51, 341 (2004)
- Ryuichi I, Yoichi T, Kazunari F, Kazushige K, Kiyoshi S, Tetsu-to-Hagane, 89(6), 699 (2003)
- Yoshikuni K, Brian FD, Malcoln M, Metall. Mater. Trans. A, 33A, 2549 (2002)
- Janovec J, Svoboda M, Blach J, Mater. Sci. Eng. A, 249, 184 (1998)
- Ennis PJ, Zielinska-Lipiec A, Wachter O, Czyrska-Filemonowicz A, Acta Metallurgica Inc., 45, 4901 (1997)
- Orlova A, Bureik J, Kucharova K, Sklenicka V, Mater. Sci. Eng. A, 245, 39 (1998)
- Hattestrand M, Andren HO, Micron, 32, 789 (2001)