Preconcentration/separation of lead at trace level from water samples by mixed micelle cloud point extraction

Nusrat Jalbani; Mustafa Soylak

Journal of Industrial and Engineering Chemistry, Vol.29, 48-51, September, 2015

DOI10.1016/j.jiec.2015.02.025 Export Citation

Preconcentration/separation of lead at trace level from water samples by mixed micelle cloud point extraction

Nusrat Jalbani^{1, 2}, and Mustafa Soylak^{1, 3, †}

¹Department of Chemistry, Fen Faculty, Erciyes University, 38039 Kayseri, Turkey
²PCSIR Laboratories, Karachi, Pakistan
³, Turkey

E-mail:

A mixed micelle-mediated cloud point extraction procedure was developed for lead. Triton-X114 and benzyldimethyl hexadecyl-ammonium chloride were used as mixed micellar medium. Lead(II) was reacted with 4-(2-pyridylazo) resorcinol at pH 6.0 to form hydrophobic chelates. The parameters including pH, ligand volume, concentrations of surfactants and centrifugation time were optimized. The effect of some common ions was also tested. The limit of detection was 1.15 mg L-1 with preconcentration factor of 50. The accuracy of method was evaluated by the analysis of certified reference materials. The method was successfully applied to determination of levels of lead in water samples.

Keywords:Mixed micelle;Cloud point formation;Pb(II);Water;Flame atomic absorption spectrometry

[References]

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Guo J, Chai Y, Yuan R, Song Z, Zou Z, Sens. Actuators B-Chem., 155, 639 (2011)
Gama EM, Lima AD, Lemos VA, J. Hazard. Mater., 136(3), 757 (2006)
Turkoglu O, Saracoglu S, Soylak M, Trace Elem. Electrolytes, 20, 225 (2003)
Gotgulu TY, Kipcak AS, Ozdemir OD, Derun EM, Piskin S, Czech J. Food Sci., 32, 555 (2014)
Freedman R, Olson L, Hoffer B, Environ. Health Perspect., 89, 27 (1990)
Jalbani N, Kazi TG, Kazi N, Jamali MK, Arain MB, Ren. Fail., 30, 737 (2008)
Percin F, Sogut O, Altinelataman C, Soylak M, Food Chem. Toxicol., 49, 1006 (2011)
Elci L, Kartal AA, Soylak M, J. Hazard. Mater., 153(1-2), 454 (2008)
Zougagh M, de Torres AG, Alonso EV, Pavon JMC, Talanta, 62, 503 (2004)
Ndung’u K, Hibdon S, Flegal AR, Talanta, 64, 258 (2004)
Acar O, Ozvatan S, Ilim M, Turk. J. Chem., 26, 335 (2005)
Mekonnen KN, Ambushe AA, Chandravanshi BS, Redi-Abshiro M, McCrindle RI, J. Environ. Sci. Health Part A-Toxic/Hazard. Subst. Environ. Eng., 50A, 90 (2015)
Soylak M, Uzun A, Elci L, Trace Elem. Electrolytes, 19, 15 (2002)
Huertas-Perez JF, Garcia-Campana AM, Anal. Chim. Acta, 630, 194 (2008)
Yilmaz E, Soylak M, Talanta, 116, 882 (2013)
Lemos VA, Teixeira LSG, Bezerra MA, Costa ACS, Castro JT, Cardodo LA, de Jesus DS, Santos ES, Baliza PX, Santos LN, Appl. Spectrosc. Rev., 43, 303 (2008)
Narin I, Soylak M, Kayakirilmaz K, Elci L, Dogan M, Anal. Lett., 36, 641 (2003)
Yurtman-Gunduz Z, Aydın-Urucu O, Kok-Yetimoglu E, Filik H, Maced. J. Chem. Chem. Eng., 32, 69 (2013)
Hinze WL, Pramauro E, Crit. Rev. Anal. Chem., 24, 133 (1993)
Samaddar P, Sen K, J. Ind. Eng. Chem., 20(4), 1209 (2014)
Hasanpour F, Alimirzaei Z, Taei M, Karimi H, Samimi R, Iran. J. Anal. Chem., 1, 44 (2014)
Narin I, Soylak M, Anal. Chim. Acta, 493, 205 (2003)
Soylak M, Elci L, Dogan M, J. Trace Microprobe Tech., 17, 149 (1999)
Elci L, Soylak M, Uzun A, Buyukpatir E, Dogan M, Fresenius J. Anal. Chem., 368, 358 (2000)
Elci A, Kabakci E, Elci L, Anal. Lett., 48, 632 (2015)
Duran A, Soylak M, Tuncel SA, J. Hazard. Mater., 155(1-2), 114 (2008)
Pourreza N, Rastegarzadeh S, Larki A, J. Ind. Eng. Chem., 20(5), 2680 (2014)
Aydin FA, Soylak M, Talanta, 72, 187 (2007)
Dadfarnia S, Shabani AMH, Amirkavei M, Turk. J. Chem., 37, 746 (2013)
Ghaedi M, Ahmadi F, Soylak M, Anal. Chim., 97, 277 (2007)
Eskandari H, Turk. J. Chem., 36, 631 (2012)
Soylak M, Dogan M, Trace Elem. Electrolytes, 13, 130 (1996)
Silva EL, Roldan PD, J. Hazard. Mater., 161(1), 142 (2009)
Sacmaci S, Kartal S, Kumsuz S, J. AOAC Int. Vol., 97, 1719 (2014)
Tuzen M, Karaman I, Citak D, Soylak M, Food Chem. Toxicol., 47, 1648 (2009)
Ghaedi M, Niknam K, Taheri K, Hosseinian H, Soylak M, Food Chem. Toxicol., 48, 891 (2010)
Bahadır Z, Bulut VN, Ozdes D, Duran C, Bektas H, Soylak M, J. Ind. Eng. Chem., 20(3), 1030 (2014)
Dhahir SA, Bakir SR, Asian J. Chem., 26, 5305 (2014)
Soylak M, Yilmaz E, Desalination, 275(1-3), 297 (2011)
Soylak M, Soylak Z, J. Ind. Eng. Chem., 20(2), 581 (2014)
Ozcan SG, Satiroglu N, Soylak M, Food Chem. Toxicol., 48, 2401 (2010)

[Referenced By]

[1] Shaw MJ, Haddad PR, Environ. Int., 30, 403 (2004)

[2] Guo J, Chai Y, Yuan R, Song Z, Zou Z, Sens. Actuators B-Chem., 155, 639 (2011)

[3] Gama EM, Lima AD, Lemos VA, J. Hazard. Mater., 136(3), 757 (2006)

[4] Turkoglu O, Saracoglu S, Soylak M, Trace Elem. Electrolytes, 20, 225 (2003)

[5] Gotgulu TY, Kipcak AS, Ozdemir OD, Derun EM, Piskin S, Czech J. Food Sci., 32, 555 (2014)

[6] Freedman R, Olson L, Hoffer B, Environ. Health Perspect., 89, 27 (1990)

[7] Jalbani N, Kazi TG, Kazi N, Jamali MK, Arain MB, Ren. Fail., 30, 737 (2008)

[8] Percin F, Sogut O, Altinelataman C, Soylak M, Food Chem. Toxicol., 49, 1006 (2011)

[9] Elci L, Kartal AA, Soylak M, J. Hazard. Mater., 153(1-2), 454 (2008)

[10] Zougagh M, de Torres AG, Alonso EV, Pavon JMC, Talanta, 62, 503 (2004)

[11] Ndung’u K, Hibdon S, Flegal AR, Talanta, 64, 258 (2004)

[12] Acar O, Ozvatan S, Ilim M, Turk. J. Chem., 26, 335 (2005)

[13] Mekonnen KN, Ambushe AA, Chandravanshi BS, Redi-Abshiro M, McCrindle RI, J. Environ. Sci. Health Part A-Toxic/Hazard. Subst. Environ. Eng., 50A, 90 (2015)

[14] Soylak M, Uzun A, Elci L, Trace Elem. Electrolytes, 19, 15 (2002)

[15] Huertas-Perez JF, Garcia-Campana AM, Anal. Chim. Acta, 630, 194 (2008)

[16] Yilmaz E, Soylak M, Talanta, 116, 882 (2013)

[17] Lemos VA, Teixeira LSG, Bezerra MA, Costa ACS, Castro JT, Cardodo LA, de Jesus DS, Santos ES, Baliza PX, Santos LN, Appl. Spectrosc. Rev., 43, 303 (2008)

[18] Narin I, Soylak M, Kayakirilmaz K, Elci L, Dogan M, Anal. Lett., 36, 641 (2003)

[19] Yurtman-Gunduz Z, Aydın-Urucu O, Kok-Yetimoglu E, Filik H, Maced. J. Chem. Chem. Eng., 32, 69 (2013)

[20] Hinze WL, Pramauro E, Crit. Rev. Anal. Chem., 24, 133 (1993)

[21] Samaddar P, Sen K, J. Ind. Eng. Chem., 20(4), 1209 (2014)

[22] Hasanpour F, Alimirzaei Z, Taei M, Karimi H, Samimi R, Iran. J. Anal. Chem., 1, 44 (2014)

[23] Narin I, Soylak M, Anal. Chim. Acta, 493, 205 (2003)

[24] Soylak M, Elci L, Dogan M, J. Trace Microprobe Tech., 17, 149 (1999)

[25] Elci L, Soylak M, Uzun A, Buyukpatir E, Dogan M, Fresenius J. Anal. Chem., 368, 358 (2000)

[26] Elci A, Kabakci E, Elci L, Anal. Lett., 48, 632 (2015)

[27] Duran A, Soylak M, Tuncel SA, J. Hazard. Mater., 155(1-2), 114 (2008)

[28] Pourreza N, Rastegarzadeh S, Larki A, J. Ind. Eng. Chem., 20(5), 2680 (2014)

[29] Aydin FA, Soylak M, Talanta, 72, 187 (2007)

[30] Dadfarnia S, Shabani AMH, Amirkavei M, Turk. J. Chem., 37, 746 (2013)

[31] Ghaedi M, Ahmadi F, Soylak M, Anal. Chim., 97, 277 (2007)

[32] Eskandari H, Turk. J. Chem., 36, 631 (2012)

[33] Soylak M, Dogan M, Trace Elem. Electrolytes, 13, 130 (1996)

[34] Silva EL, Roldan PD, J. Hazard. Mater., 161(1), 142 (2009)

[35] Sacmaci S, Kartal S, Kumsuz S, J. AOAC Int. Vol., 97, 1719 (2014)

[36] Tuzen M, Karaman I, Citak D, Soylak M, Food Chem. Toxicol., 47, 1648 (2009)

[37] Ghaedi M, Niknam K, Taheri K, Hosseinian H, Soylak M, Food Chem. Toxicol., 48, 891 (2010)

[38] Bahadır Z, Bulut VN, Ozdes D, Duran C, Bektas H, Soylak M, J. Ind. Eng. Chem., 20(3), 1030 (2014)

[39] Dhahir SA, Bakir SR, Asian J. Chem., 26, 5305 (2014)

[40] Soylak M, Yilmaz E, Desalination, 275(1-3), 297 (2011)

[41] Soylak M, Soylak Z, J. Ind. Eng. Chem., 20(2), 581 (2014)

[42] Ozcan SG, Satiroglu N, Soylak M, Food Chem. Toxicol., 48, 2401 (2010)