화학공학소재연구정보센터
Applied Surface Science, Vol.390, 167-174, 2016
Influence of surface morphology and microstructure on performance of CVD tungsten coating under fusion transient thermal loads
Thick tungsten coatings have been deposited by chemical vapor deposition (CVD) at a rapid growth rate. A series of tungsten coatings with different thickness and surface morphology were prepared. The surface morphology, microstructure and preferred orientation of the CVD tungsten coatings were investigated. Thermal shock analyses were performed by using an electron beam facility to study the influence of the surface morphology and the microstructure on the thermal shock resistance of the CVD tungsten coatings. Repetitive (100 pulses) ELMs-like thermal shock loads were applied at various temperatures between room temperature and 600 degrees C with pulse duration of 1 ms and an absorbed power density of up to 1 GW/m(2). The results of the tests demonstrated that the specific surface morphology and columnar crystal structure of the CVD tungsten have significant influence on the surface cracking threshold and crack propagation of the materials. The CVD tungsten coatings with a polished surface show superior thermal shock resistance as compared with that of the as-deposited coatings with a rough surface. (C) 2016 Elsevier B.V. All rights reserved.