Journal of Industrial and Engineering Chemistry, Vol.47, 51-55, March, 2017
Synthesis of self-assembled rectangular-shaped polyaniline nanotubes and their physical characteristics
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We reports synthesis of polyaniline (PANI) nanotubes with a rectangular cross-sectional shape by simply changing both molar ratio of organic dopant acid to monomer and reaction time. The PANI nanotubes were fabricated with a controlled rectangular pore structure by an in-situ chemical oxidation polymerization process in the absence of surfactant and template. Morphology of citric acid (CA)-doped PANI was observed via scanning electron microscopy and transmission electron microscopy. Fourier transform infrared spectroscopy and X-ray diffraction confirmed chemical structure and hydrogen bonding between amine group of PANI and hydroxyl and carboxyl group of CA, is the driving force for this self-assembly.
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