Chemical Engineering and Processing, Vol.113, 56-64, 2017
Continuous flow-microwave reactor: Where are we?
This article presents the different microwave continuous reactors existing, which are reported in literature to carry out chemical synthesis with a more efficient way. It shows how the methods and tools of chemical engineering can be useful and necessary to define, characterize and optimize the microwave reactors. This review scans continuous microwave reactors, by describing the different types of microwave technologies used (multimode, single-mode, coaxial or guided transmission...). It then focuses on the various existing reactor geometries and on the control of the electromagnetic field homogeneity. The problem of temperature measurement and overall instrumentation is also addressed (input power, reflected power, continuous adaptation...). This review scans the most efficient microwave continuous flow reactors existing in the literature and highlights how the microwave technology is used as well as chemical engineering tools. It points out the reactors geometries, the control of the electromagnetic field and the measurement of the physical parameters (Temperature, microwave power, etc.). Finally, the scale-up of continuous-flow microwave reactors is examined through the existing lab-scale and semi industrial pilot plants described in literature. (C) 2016 Elsevier B.V. All rights reserved.