Identification of phosphorus forms in sewage sludge ash during acid pre-treatment for phosphorus recovery by chemical fractionation and spectroscopy

Minsu Lee; Dong-Jin Kim

Journal of Industrial and Engineering Chemistry, Vol.51, 64-70, July, 2017

DOI10.1016/j.jiec.2017.02.013 Export Citation

Identification of phosphorus forms in sewage sludge ash during acid pre-treatment for phosphorus recovery by chemical fractionation and spectroscopy

Minsu Lee, and Dong-Jin Kim^†

Department of Environmental Sciences & Biotechnology and Institute of Energy & Environment, Hallym University, 1 Okchon, Chuncheon, Gangwon 200-702, Republic of Korea

E-mail:

Identification of phosphorus (P) forms is critical for the recovery of P from sewage sludge ash (SSA). During the HCl treatment of SSA Ca was selectively eluted while P mostly remained in the SSA. Chemical P fractionation of the SSA before and after HCl treatment showed that Al-P increased from 46.6% to 79.2% of total P while Ca-P decreased from 28.9% to 4.4% at pH 2.5. HCl treatment also changed chemical structure of Al-P since no crystalline Al-P was found in the SSA after the treatment, only amorphous Al-P was found from the analyses of XRD and ATR-FTIR.

Keywords:Acid pre-treatment;Chemical fractionation;Identification of phosphorus compounds;Phosphorus recovery;Sewage sludge ash

[References]

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[Referenced By]

[1] Cooper J, Lombardi R, Boardman D, Marquet CC, Resour. Conserv. Recycl., 57, 78 (2011)

[2] Kim M, Han DW, Kim DJ, Bioresour. Technol., 190, 522 (2015)

[3] Ali TU, Kim DJ, Bioresour. Technol., 217, 233 (2016)

[4] Adam C, Peplinski B, Michaelis M, Kley G, Simon FG, Waste Manage., 29, 1122 (2009)

[5] Gustafsson JP, Visual MINTEQ. Ver. 3.0, (2012) . http://vminteq.lwr.kth.se/.

[6] Donatello S, Tong D, Cheeseman CR, Waste Manage., 30, 1634 (2010)

[7] Petzet S, Peplinski B, Bodkhe SY, Cornel P, Water Sci. Technol., 64, 693 (2011)

[8] Lim BH, Kim DJ, J. Ind. Eng. Chem., 46, 62 (2017)

[9] Paludan C, Jensen HS, Wetlands, 15, 365 (1995)

[10] Mazur EB, Mazur A, Stoinska R, Environ. Prot. Eng., 40, 161 (2014)

[11] Anderson KJ, Kisser MI, Horizontal 6 (2004).

[12] Franson MAH, Eaton AD, Clesceri LS, Rice EW, Greenberg AE, APHA, 21, 4 (2008)

[13] Miller FA, Wilkins CH, Anal. Chem., 24, 1253 (1952)

[14] Vogel C, Kohl A, Adam C, Appl. Spectrosc., 65, 265 (2011)

[15] Elzinga EJ, Sparks DL, J. Colloid Interface Sci., 308(1), 53 (2007)

[16] Donatello S, Cheeseman CR, Waste Manage., 33, 2328 (2013)

[17] Huang X, Foster GD, Honeychuck RV, Schreifels JA, Langmuir, 25(8), 4450 (2009)

[18] Hem SL, Burrell LS, Johnston CT, Schulze D, Klein J, White JL, Vaccine, 19, 275 (2000)

[19] Galebeck F, Rosseto R, Santos A, Braz J, Chem. Soc. Rev., 17, 1465 (2006)

[20] Ambrosio AMA, Sahota JS, Khan Y, Laurencin CT, J. Biomed. Mater. Res., 58, 295 (2001)

[21] Roncal-Herrero T, Rodriguez-Blanco JD, Bennig LG, Oelkers EH, Growth Des., 9, 5197 (2009)

[22] Christie DM, Troullier N, Chelikowsky JR, Solid State Commun., 98, 923 (1996)

[23] Lagno F, Demopoulos GP, Ind. Eng. Chem. Res., 44(21), 8033 (2005)

[24] Li W, Feng J, Kwon KD, Kubicki JD, Phillips BL, Langmuir, 26(7), 4753 (2010)

[25] Tandy S, Healey JR, Nason MA, Williamson JC, Jones DL, Thain SC, Bioresour. Technol., 101(14), 5431 (2010)

[26] Kaikake K, Sekito T, Dote Y, Waste Manage., 29, 1084 (2009)

[27] Rokita M, Handke M, Mozgawa W, J. Mol. Struct., 511-512, 277 (1999)

[28] Friedrich F, Weidler PG, Appl. Spectrosc., 64, 500 (2010)

[29] Wendling LA, Blomberg P, Sarlin T, Priha O, Arnold M, Geochemical, 7, 157 (2013)

[30] Zheng TT, Sun ZX, Yang XF, Holmgren A, Chem. Cent. J., 6, 26 (2012)