Currently, general aviation aircrafts have growing demand for internal combustion engines burning heavy fuels (i. e. diesel or kerosene) due to the concerns on the safety, costs and availability of aviation gasoline (AVGAS). The application of heavy fuels requires the change of combustion mode from premixed mode to diffusion mode, which will inevitably increase the particulate matter (PM) emissions as incomplete combustion products. In this work, the size-resolved number concentrations of the PM emissions emitted from an internal compression ignition engine burning diesel, RP3 and FischerTropsch (FT) kerosene were studied by a Scanning Mobility Particle Sizer Spectrometer (SMPS). An opacimeter was utilized to measure the opacity of the soot emissions (linearly related to the soot mass), which was in consistent with the SMPS data. Results demonstrated that the FT fuel produced the lowest PM emissions due to absence of sulfur and aromatic contents. Diesel turned out to have the greatest ` sooting' tendency and produced more accumulation mode PM in number than FT fuel by a factor of four, and more PM in mass by approximately three times. Moreover, the effects of fuel types and engine operational parameters were quantified in a systematic manner by adopting the Response Surface Method (RSM) in Design of Experiments (DoE). According to the ANOVA (Analysis of Variance), the DoE derived model was statistically significant and demonstrated that the engine load was the dominant factor for soot generation, followed by injection pressure and fuel types. Relevant combustion parameters and their link with PM emissions were further discussed, illustrating that atomization process had great impact on the ignition delay and thus affected soot generation. (C) 2017 Elsevier Ltd. All rights reserved.