디스펜서 프린팅을 위한 ZrO2 세라믹 잉크의 합성 및 특성 평가

이지현; 황해진; 김진호; 황광택; 한규성; Ji-Hyeon Lee; Hae-Jin Hwang; Jin-Ho Kim; Kwang-Taek Hwang; Kyu-Sung Han

Korean Journal of Materials Research, Vol.28, No.2, 95-100, February, 2018

DOI10.3740/MRSK.2018.28.2.95 Export Citation

디스펜서 프린팅을 위한 ZrO2 세라믹 잉크의 합성 및 특성 평가

Synthesis and Characterization of ZrO2 Ceramic Ink for Dispenser Printing

이지현^{1, 2}, 황해진², 김진호¹, 황광택¹, 한규성^{1, †}

¹한국세라믹기술원 도자세라믹센터
²인하대학교 신소재공학과

Ji-Hyeon Lee^{1, 2}, Hae-Jin Hwang², Jin-Ho Kim¹, Kwang-Taek Hwang¹, and Kyu-Sung Han^{1, †}

¹Ceramic ware Center, Korea Institute of Ceramic Engineering and Technology, Icheon 17303, Republic of Korea
²Division of Material Science and Engineering, Inha University, Incheon 22212, Republic of Korea

E-mail:

In this study, ZrO2 ceramic ink was formulated for additive manufacturing three dimensional structure using dispenser printing technique. Ceramic ink with various ZrO2 loading (30, 40, 50vol%) was prepared to evaluate their rheological properties and printability. High ZrO2 loading ZrO2 ceramic ink showed higher elastic modulus and improved shape retention, when the ceramic ink was printed and sintered at 1450 °C for 1h. Microstructural analysis of printed ZrO2 objective indicated that high ZrO2 loading objective showed lower porosity and smaller pore size.

Keywords:additive manufacturing;ZrO2;ceramic ink;dispenser printing;raw material

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[1] Denry I, Kelly JR, Dent. Mater., 24, 299 (2008)

[2] Hannink RHJ, Kelly PM, Muddle BC, J. Am. Ceram. Soc., 83(3), 461 (2000)

[3] Piconi C, Maccauro G, Biomaterials, 20, 1 (1999)

[4] Calvert P, Crockett R, Chem. Mater., 9, 650 (1997)

[5] Dimas LS, Bratzel GH, Eylon I, Buehler MJ, Adv. Funct. Mater., 23, 4629 (2013)

[6] Griffith ML, Halloran JW, J. Am. Ceram. Soc., 79, 2601 (1996)

[7] Liu K, Sun H, Tan Y, Shi Y, Liu J, Zhang S, Huang S, Int. J. Adv. Manuf. Technol., 90, 945 (2017)

[8] Griffin C, Daufenbach J, McMillin S, Am. Ceram. Soc. Bull., 73, 109 (1994)

[9] Kalita SJ, Bose S, Hosick HL, Bandyopadhyay A, Mater. Sci. Eng. C-Biomimetic Supramol. Syst., 23, 611 (2003)

[10] Fu QA, Saiz E, Tomsia AP, Adv. Funct. Mater., 21(6), 1058 (2011)

[11] Tubio CR, Guitian F, Gil A, J. Eur. Ceram. Soc., 36, 3409 (2016)

[12] Compton BG, Lewis JA, Adv. Mater., 26(34), 5930 (2014)

[13] Smay JE, Cesarano J, Lewis JA, Langmuir, 18(14), 5429 (2002)

[14] Conrad JC, Ferreira SR, Yoshikawa J, Shepherd RF, Ahn BY, Lewis JA, Curr. Opin. Colloid Interface Sci., 16, 71 (2011)

[15] Ahn BY, Duoss EB, Motala MJ, Guo X, Park S, Xiong Y, Yoon J, Nuzzo RG, Rogers JA, Lewis JA, Science, 323, 1590 (2009)

[16] Sun C, Wu T, Liu R, Liang B, Tian Z, Zhang E, Zhang M, Food Hydrocolloids, 51, 512 (2015)

[17] Pasqua A, Fleury M, Brun A, Cristiano MC, Cosco D, Adv. Food Safety Health, 6, 61 (2014)

[18] Xu D, Zhang J, Cao Y, Wang J, Xiao J, LWTFood Sci. Technol., 66, 590 (2016)

[19] Sim KJ, Youn HJ, Ahn JE, Lee JG, Lee HY, Jo YH, J. Korea TAPPI, 46, 46 (2014)

[20] Hazan YD, Thanert M. Trunec M, Misak J, J. Eur. Ceram. Soc., 32, 1187 (2012)