Utilization of a triacetylcellulose membrane to immobilize5-(2',4'-dimethylphenylazo)-6-hydroxypyrimidine-2,4-dione for erbium determination in real samples

Zakia Al-Mallah; Alaa S. Amin

Journal of Industrial and Engineering Chemistry, Vol.63, 281-287, July, 2018

DOI10.1016/j.jiec.2018.02.027 Export Citation

Utilization of a triacetylcellulose membrane to immobilize5-(2',4'-dimethylphenylazo)-6-hydroxypyrimidine-2,4-dione for erbium determination in real samples

Zakia Al-Mallah, and Alaa S. Amin^{1, †}

Chemistry Department, Faculty of Science, Umm-Quarh University, Saudi Arabia
¹Chemistry Department, Faculty of Science, Benha University, Benha, Egypt

E-mail:

A membrane optode formed by physical inclusion of a chromophore 2-amino-6-(1,3-thiazol-2yldiazenyl) phenol (ATDP) into a plasticized cellulose triacetate (CTA) matrix was investigated for preconcentration, extraction and colorimetric determination of Er(III) from aqueous samples. The optode was examined for erbium uptake in borate buffer medium (~125 ng mL-1) at pH 8.5.9.0. The inclusion of an anionexchanger tri-isooctylamine (TiOA) was found to be necessary for the formation of Er(III)-ATDP complex in the optode matrix, resulting into distinct color change of the optode from red to violet color after erbium sorption. The composition of the optode was prepared by varying the amounts of different plasticizers and TiOA to obtain minimum response time towards Er(III) in borate buffer medium. The effects of different experimental parameters involved in the detection and quantification of Er(III) using optode were optimized. The optode analytical performance was performed in terms of interference of cations and anions, reusability, equilibration time, detection limit, etc. and compared with the conventional colorimetric method for Er(III) using different chromophores. The optode developed in the present study was tested in real samples with good results comparing to the GF-AAS method.

Keywords:Erbium(VI) determination;Membrane optode;Visual colorimetry;2-Amino-6-(1,3-thiazol-2yldiazenyl);phenol;Environmental analysis

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[2] Li Y, Yang JL, Jiang Y, J. Agric. Food Chem., 60, 3033 (2012)

[3] Tucher SV, Goy C, Schmidhalter U, et al. Kluwer Academic Publishers, Dordrecht, The Netherlands, p.524 2001.

[4] Buckingham S, Maheswaran J, Meehan B, Peverill K, Mater. Sci. Forum, 315, 339 (1999)

[5] Zhu HD, Wu Q, Fan TJ, Liu QF, Zhang W, J. Radiol. Prot., 28, 573 (2008)

[6] Chen ZY, Zhu XD, J. Ecol. Rural Environ., 24, 88 (2008)

[7] Bhaktha SNB, Boulard B, Chaussedent S, Chiappini A, Chiasera A, Duval E, et al., Opt. Mater., 28, 1325 (2006)

[8] Fine LW, Beall H, Chemistry for Engineers and Scientists, Saunders College publishing, Philadelphia, 1990.

[9] Morison GH (Ed.), Trace Analysis Physical Methods, John Wiley & Sons, New York, 1965.

[10] Cheng J, Chen W, Chen G, Opt. Laser Technol., 78, 71 (2016)

[11] Anbu M, Rao TP, Iyer CSP, Damodaran AD, Chem. Anal. (Warsaw), 41, 781 (1996)

[12] Wang NX, Si ZK, Yang JH, Du AQ, Talanta, 43, 589 (1996)

[13] Wang NX, Yang JH, Siu H, Qi P, Analyst, 120, 2413 (1995)

[14] Holzbrecher H, Brever U, Gastel M, Becker JS, Dietze HJ, Beckers I, Bauer S, Elenster M, Zander W, Schubeat J, Buehar C, J. Anal. Chem., 383, 785 (1995)

[15] Perina V, Vaick J, Hnatowicz V, Cerena J, Kolarova P, SpirkovaHeradilova J, Schrofel J, Nucl. Instrum. Methods Phys. Res. B, 139, 208 (1998)

[16] Bandi KR, Upadhyay A, Singh AK, Jain AK, Mater. Sci. Eng. C-Biomimetic Supramol. Syst., 62, 9 (2016)

[17] Marczenko Z, Spectrophotometric Determination of Elements, Ellis Horwood, Chichester, 1976.

[18] Elchuk S, Cassidy R, Anal. Chem., 51, 1434 (1979)

[19] Wolsfsberg A, Anal. Chem., 34, 518 (1962)

[20] Martinez L, Perino E, Marchevsky E, Oksina R, Talanta, 40, 385 (1993)

[21] Ganjalia MR, Hosseini M, Hariri M, Faridbod F, Norouzi P, Sens. Actuators B-Chem., 142, 90 (2009)

[22] Oehme I, Wolfbies OS, Mikrochim. Acta, 126, 177 (1997)

[23] Joannon S, Telouk P, Pin C, Spectrochim. Acta B, 52, 1783 (1997)

[24] Steinberg IM, Lobnik A, Wolfbies OS, Sens. Actuators B-Chem., 90, 230 (2003)

[25] Lerchi M, Bakker E, Rusterholz B, Simon W, Anal. Chem., 64, 1534 (1992)

[26] Mohr GJ, Wolbeis OS, Anal. Chim. Acta, 292, 41 (1994)

[27] Capitan-Vallvey LF, Ramos MDF, Galvez PADC, Gomez J, Talanta, 65, 239 (2005)

[28] Bakker E, Buhlmann P, Pretsch E, Chem. Rev., 97(8), 3083 (1997)

[29] Buhlmann P, Pretsch E, Bakker E, Chem. Rev., 98(4), 1593 (1998)

[30] Wolfbeis OS, Anal. Chem., 78, 269 (2004)

[31] Scindia YM, Pandey AK, Reddy AVR, Manohar SB, Anal. Chim. Acta, 515, 311 (2004)

[32] Sodaye S, Tripathi R, Pandey AK, Reddy AVR, Anal. Chim. Acta, 514, 159 (2004)

[33] Plaschke M, Czolk R, Ache HJ, Anal. Chim. Acta, 304, 107 (1995)

[34] Murkovic I, Wolfbeis OS, Sens. Actuators B-Chem., 38-39, 246 (1997)

[35] Ryabchikov D, Ryabukhin V, Ann Arbor-Humphrey Science Pub, London, 1970.

[36] Amin AS, El-Sheikh R, Shaltout MI, Canad. Chem. Trans., 3, 171 (2015)

[37] Britton HTS, Hydrogen Ions, 4th edn., Chapman and Hall, London, 1952.

[38] Stary J, The Solvent Extraction of Metal Chelates, Pergamon Press, New York, 1964.

[39] Story JN, Fritz JS, Talanta, 21, 892 (1974)

[40] Sodaye S, Suresh G, Pandey AK, Goswami A, Radiochim. Acta, 94, 347 (2006)

[41] Silva MF, Fernandez L, Olsina RA, Stacchiola D, Anal. Chim. Acta, 342, 229 (1997)

[42] D’Angelo J, Fernandez J, Martinez L, Marchevsky EJ, J. Anal. Chem., 54, 665 (1999)

[43] Suva MF, Fernandez LP, Olsina RA, Anal. Quim., 92, 344 (1996)

[44] Mendez JH, Cordero BM, Perez-Pavon JL, Talanta, 35, 293 (1988)

[45] Wang NX, Yang JH, Siu H, Qi P, Analyst, 120, 2413 (1995)

[46] Wang NX, Wang L, Jiang W, Qi P, Fresenius J. Anal. Chem., 361, 821 (1998)

[47] Miller JN, Miller JC, Statistics and Chemometrics for Analytical Chemistry, 5th ed., Prentice Hall, England, 2005.