Journal of Industrial and Engineering Chemistry, Vol.67, 255-265, November, 2018
Distillation design and optimization of quaternary azeotropic mixtures for waste solvent recovery
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The huge amount of solvents used in the semi-conductor and display industry typically result in waste of valuable solvents which often form complex azeotropic mixtures. This study explored a recovery process of a quaternary waste solvent, comprising methyl 2-hydroxybutyrate, propylene glycol monomethyl ether acetate, ethyl lactate, and ethyl-3-ethoxy propionate. In this study, a novel shortcut column method with a graphical approach was exploited for the distillation column design of complex quaternary azeotropic mixtures. As a result, the proposed shortcut method and design procedure solved the complex separation paths successfully with less computational efforts while achieving all requirements for component purity.
Keywords:Waste solvent recovery;Propylene glycol monomethyl ether acetate;Ethyl lactate;Quaternary azeotropic mixture;Short-cut column method
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