Quality control of Li1+delta Mn2-delta O4 spinels with their impurity phases by Jaeger and Vetter titration

Kelder EM; Jak MJG; Schoonman J; Hardgrave MT; de-Andersen SY

Journal of Power Sources, Vol.68, No.2, 590-592, 1997

DOI10.1016/S0378-7753(96)02568-2 Export Citation

Quality control of Li1+delta Mn2-delta O4 spinels with their impurity phases by Jaeger and Vetter titration

Kelder EM, Jak MJG, Schoonman J, Hardgrave MT, de-Andersen SY

Powders of lithium manganese oxide phases are synthesised and characterised for possible application in a Li-ion battery. A modified phase diagram on the basis of the manganese oxidation state and content is used to interpret the results. X-ray diffraction, flame atomic absorption spectroscopy, and Jaeger and Vetter titration are performed in order to classify the synthesised powders. The experiments reveal powders of Li1+deltaMn2-deltaO4 (0

Keywords:MANGANESE