Inorganic Chemistry, Vol.57, No.15, 8705-8708, 2018
Facile Preparation of Haggite by Reducing V2O5 in Guaiacol/ Methanol Solution
Haggite-structured V4O6(OH)(4) is prepared via a one-step reduction of V2O5 in a mixture of guaiacol and methanol. Guaiacol delays the overreduction of Haggite to V2O3 . The time window for the stable existence of the Haggite phase is enlarged at low temperature.