화학공학소재연구정보센터
Journal of Industrial and Engineering Chemistry, Vol.76, 245-250, August, 2019
A novel process for simultaneous degumming and deacidification of Soybean, Canola and Sunflower oils by tetrabutylphosphonium phosphate ionic liquid
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In this study simultaneous degumming and deacidification of edible oils were done by tetrabutylphosphonium phosphate IL. Under the optimized extraction conditions of soybean oil (3 mass% IL, 60 °C and 20 min), canola oil (2 mass% IL, 60 °C and 20 min) and sunflower oil (1.5 mass% IL, 50 °C, 15 min), the content of free fatty acid (FFA) and phosphorus reached 0.18% and 3.5 mg/kg; 0.12% and 3.8 mg/kg; and 0.17% and 3.5?mg/kg, respectively. In this work, soap stock and water washing stage were eliminated and no waste water, which pollutes the environment, was produced.
  1. Mohsen-Nia M, Dargahi M, J. Chem. Eng. Data, 52(3), 910 (2007)
  2. Bhosle BM, Subramanian R, J. Food Eng., 69(4), 481 (2005)
  3. Gimeno E, Castellote AI, Lamuela-Raventos RM, Torre MC, Lopez-Sabater MC, J. Chromatogr. A, 881, 251 (2000)
  4. Wang X, Wang X, Wang T, J. Ind. Eng. Chem., 48, 119 (2017)
  5. Shahidi F, Bailey’s Industrial Oil and Fat Products, sixth ed., John Willey and sons, New Jersey, 2005.
  6. O’Brien RD, Fats and Oils Formulating and Processing for Application, third ed., CRC Press, New York, 2009.
  7. Manic MS, Visak VN, Ponte MN, Visak ZP, AlChE J., 57, 1344 (2011)
  8. Manjula S, Subramanian R, Crit. Rev. Food Sci. Nutr., 46, 569 (2006)
  9. Verleyen T, Sosinska U, Ioannidou S, Verhe R, Dewettinck K, Huyghebaert A, De Greyt W, J. Am. Oil Chem. Soc., 79, 947 (2002)
  10. Dijkstra AJ, Eur. J. Lipid Sci. Technol., 112, 1178 (2010)
  11. Subramanian R, Nakajima M, J. Am. Oil Chem. Soc., 74, 971 (1997)
  12. Ochoa N, Pagliero C, Marchese J, Mattea M, Sep. Purif. Technol., 22, 417 (2001)
  13. Saravanan M, Bhosle BM, Subramanian R, J. Food Eng., 74(4), 529 (2006)
  14. Blahusiak M, Schlosser S, Martak J, Sep. Purif. Technol., 119, 102 (2013)
  15. Sharma P, Gupta M, J. Chem. Sci., 128, 61 (2016)
  16. Zhang Y, Li T, Wu ZK, Yu P, Luo YB, J. Chem. Thermodyn., 74, 209 (2014)
  17. Yao C, Pitner WR, Anderson JL, Anal. Chem., 81, 5054 (2009)
  18. Bara JE, Gabriel CJ, Lessmann S, Carlisle TK, Finotello A, Gin DL, Noble RD, Ind. Eng. Chem. Res., 46, 3580 (2007)
  19. Chen SH, Zhao Q, Xu XW, J. Chem. Sci., 120, 481 (2008)
  20. Marsh KN, Boxall JA, Lichtenthaler R, Fluid Phase Equilib., 219(1), 93 (2004)
  21. Anderson K, Goodrich P, Hardacre C, Hussain A, Rooney DW, Wassell D, Fuel, 108, 715 (2013)
  22. Calvano CD, De Ceglie C, D’Accolti L, Zambonin CG, Food Chem., 134, 1192 (2012)
  23. Birdwell JF, McFarlane J, Hunt RD, Luo HM, DePaoli DW, Sep. Sci. Technol., 41(10), 2205 (2006)
  24. Zhou Q, Bai H, Xie G, Xiao J, J. Chromatogr. A, 1177, 43 (2008)
  25. Zhou Q, Bai H, Xie G, Xiao J, J. Chromatogr. A, 1188, 148 (2008)
  26. Zhao Q, Zhang X, Xiao J, J. Chromatogr. A, 1216, 4361 (2009)
  27. Baghdadi M, Shemirani F, Anal. Chim. Acta, 634, 186 (2009)
  28. Aathira MS, Khatri PK, Jain SL, J. Ind. Eng. Chem., 64, 420 (2018)
  29. Hwang S, Park Y, Park K, J. Chem. Thermodyn., 43(3), 339 (2011)
  30. Safarov J, Kul I, El-Awady WA, Nocke J, Shahverdiyev A, Hassel E, J. Chem. Thermodyn., 51, 82 (2012)
  31. Vakili-Nezhaad G, Vatani M, Asghari M, Ashour I, J. Chem. Thermodyn., 54, 148 (2012)
  32. Alvarez VH, Mattedi S, Aznar M, Ind. Eng. Chem. Res., 51(44), 14543 (2012)
  33. Gomez E, Calvar N, Dominguez A, Macedo EA, J. Chem. Thermodyn., 42(11), 1324 (2010)
  34. Ramnial T, Ino DD, Clyburne JAC, Chem. Commun., 3, 325 (2005)
  35. Del Sesto RE, Corley C, Robertson A, Wilkes JS, J. Organomet. Chem., 690, 2536 (2005)
  36. Cieniecka-Rosonkiewicz A, Pernak J, Kubis-Feder J, Ramani A, Robertson AJ, Seddon KR, Green Chem., 7, 855 (2005)
  37. Kagimoto J, Fukumoto J, Ohno H, Chem. Commun., 21, 2254 (2006)
  38. Welton T, Chem. Rev., 99(8), 2071 (1999)
  39. Firestone D, Official Methods and Recommended Practices of American Oil Chemists’ Society. Method Ca 5a-40, (2012).
  40. Firestone D, Official Methods and Recommended Practices of American Oil Chemists’ Society. Method Ca 12-55, (2009).