We report the first investigation of zirconyl 2-ethyl hexanoate micelles in decane using small-angle neutron and X-ray scattering. Our results show that the micelles have a spherical shell structure consisting of an inner core region with a radius of 6.3 Angstrom that is surrounded by a shell 5.3 Angstrom thick incorporating the surfactant chain segments. From the contrast variation experiment, we calculated there were 33 surfactant molecules/micelle. Finally, our small-angle neutron scattering experiments performed at 80 degrees C showed there was no change in the shape or size of the micelles at the higher temperature.