화학공학소재연구정보센터
Journal of Vacuum Science & Technology B, Vol.24, No.3, 1081-1087, 2006
Characterizing field emission from individual carbon nanotubes at small distances
This article demonstrates the characterization of field emission from individual carbon nanotubes (CNTs) attached to a tungsten tip, when the separation distance s between the anode and tip of the CNT (cathode) is less than 15 mu m. The separation distance is adjusted with a nanopositioning stage after establishing a datum by detecting the anode surface with the CNT tip. Our separation distance s differs by the height h of the. CNT from the distance d that is often measured between the planar anode and the planar substrate of an emitting cathode. Consequently, the electric field at the tip of the CNT is modeled by F=lambda V/s, where h is our field amplification factor, rather than by F=gamma V/d, where gamma is the more conventional field enhancement factor. Twenty-four sets of current-voltage I(V) data were measured from an individual multiwall CNT at separation distances s between 1.4 and 13.5 mu m. A nonlinear curve-fitting algorithm extracted Fowler-Nordheim (FN) parameters from each set of I(V) data, rather than conventional extraction from the FN plots. The turn-on voltage V-to (to emit 1 nA) as a function of the separation distance followed an empirical power relation V-to=as(b), and the field amplification factor X empirically followed the relation lambda=lambda(proportional to)s/(s+h)+1. This experimental characterization is an improvement over other techniques since the gap is controlled more precisely over a larger range, the electric field at the CNT tip is not disturbed by other CNTs, and the anode is flat to within a few nanometers. (c) 2006 American Vacuum Society.