Thin Solid Films, Vol.513, No.1-2, 217-222, 2006
Coating of carbon short fibers with thin ceramic layers by chemical vapor deposition
Carbon short fiber bundles with a length of 6 mm were uniformly coated using specially designed, continuous chemical vapor deposition (CVD) equipment. Thin layers of titanium nitride, silicon nitride (SiC) and pyrolytic carbon (pyC) were deposited onto several kilograms of short fibers in this large scale CVD reactor. Thermo-gravimetric analyses and scanning electron microscopy investigtions revealed layr thicknesses between 20 and 100nm on the fibers. Raman spectra of pyC coated fibers show a change of structural order depending on the CVD process parameters. For the fibers coated with SiC, Raman investigations showed a deposition of amorphous SiC. The coated carbon short fibers will be applied as reinforcing material in composites with ceramic and metallic matrices. (c) 2006 Elsevier B.V. All rights reserved.
Keywords:chemical vapor deposition;carbon fibers;pyrolytic carbon;titanium nitride;silicon carbide;scanning electron microscopy