화학공학소재연구정보센터
Journal of the American Ceramic Society, Vol.83, No.5, 1199-1206, 2000
Fracture resistance and stable crack-growth behavior of 8-mol%-yttria-stabilized zirconia
The crack-growth behavior of a yttria-stabilized zirconia ceramic (8 mol% of cubic-phase yttria) was studied at room temperature. Double-cantilever-beam specimens were loaded with pure bending moments in a specially designed loading fixture inside an environmental scanning electron microscope. Crack-growth data were obtained from truly sharp (arrested) cracks, bypassing interpretation problems that involve crack initiation from a machined notch. The crack-growth study was conducted over a range of applied energy-release rates that allowed crack arrest on one hand and fast fracture on the other. Three energy-release-rate values were relevant initiation of crack growth (3.5 J/m(2)), crack arrest (2.8 J/m(2)), and fast fracture (8.0 J/m(2)). At the macroscopic scale, subcritical crack growth occurred as a continuous process. In situ observations revealed that, at the microscopic scale, crack growth occurred in small jumps. The fracture mode for stable crack growth was identified to be transgranular.