Journal of the American Ceramic Society, Vol.86, No.1, 39-42, 2003
Fabrication of silicon carbide-mullite composite by melt infiltration
The melt infiltration method was used to fabricate a SiC-mullite composite at high temperature. Mullite was successfully obtained from a SiO2 and Al2O3 powder mixture by melting above 1830degreesC in a BN crucible with a lid. When infiltrated into a porous SiC preform, the mullite significantly reacted with SiC to form gaseous SiO and CO, even at the lowest investigated temperature of 1830degreesC, consuming SiO2 and leaving Al2O3 and silicon phases in the sample. The relevant reactions were studied in detail. A closed system was adopted to suppress the reaction, and a dense composite was successfully obtained.