Journal of the American Ceramic Society, Vol.86, No.5, 811-816, 2003
Nanoindentation method for measuring residual stress in brittle materials
The lowered threshold load for cracking with the cube-corner indenter has been used in developing a method that can be used to measure residual stresses in small volume brittle materials. By studying a series of orthogonal cracks generated at loads not exceeding 10 mN with the cube-corner indenter, a variation of crack length with position around a large Vickers impression in soda-lime glass was observed. Using an indentation fracture mechanics approach residual stresses were evaluated at the positions where the cube-corner indents had been made. The stress values thus evaluated were generally higher than those reported in the literature where micro-Vickers indents had been used to measure the stresses. Possible reasons for the disparity are discussed.