Materials Chemistry and Physics, Vol.69, No.1-3, 278-280, 2001
Simple synthetic method for MSe2 (M=Fe, Co or Ni) nanocrystallites at low temperature
A simple solventothermal method has been employed for nanocrystalline MSe2 (M=Fe, Co or Ni) at 160 degreesC. The final product phases were confirmed by X-ray diffraction (XRD). Transmission electron microscopy (TEM) revealed that the obtained crystalline MSe2 consist of nano-particles and a small amount of irregular plate-like products with relatively large size.