화학공학소재연구정보센터
Macromolecular Research, Vol.16, No.2, 163-168, February, 2008
Fabrication and Characterization of Polystyrene/Gold Nanoparticle Composite Nanofibers
E-mail:
Polystyrene/gold nanoparticle (PS/AuNP) composite fibers were fabricated using an electrospinning technique. Transmission electron microscopy (TEM) showed that the diameters of the naphthalenethiol-capped gold nanoparticles (prior to incorporation into the PS fibers) ranged from 2 to 5 nm. UV-vis spectroscopy revealed the surface plasmon peaks of the gold nanoparticles centered at approximately 512 nm, indicating that nano-sized Au particles are well-dispersed in solution. This was consistent with the TEM observations. The electrospun nanofibers of PS/AuNP composites were approximately 60-3,000 nm in diameter. The surface morphology of the PS/AuNP composite and the dispersability of the Au nanoparticles inside of PS after electrospinning process were investigated by SEM and TEM. The thermal behavior of the pure PS and PS/AuNP nanocomposites and fibers were examined by DSC.
  1. Heiz U, Landman U, Nanocatalysis, Springer, Berlin (2007)
  2. Lau KHA, Knoll W, Kim DH, Macromol. Res., 15(3), 211 (2007)
  3. Frolov GI, Tech. Phys., 46, 1537 (2001)
  4. Shemer G, Markovich G, J. Phys. Chem. B, 106(36), 9195 (2002)
  5. Aktsipetrov OA, Colloids Surf. A: Physicochem. Eng. Asp., 202, 165 (2002)
  6. Menendez JL, Bescos B, Armelles G, Serna R, Gonzalo J, Doole R, Petford-Long AK, Alonso MI, Phys. Rev. B, 65, 205413 (2002)
  7. Kharitonov AB, Shipway AN, Willner I, Anal. Chem., 71, 5441 (1999)
  8. Kharitonov AB, Shipway AN, Katz E, Willner I, Rev. Anal. Chem., 18, 255 (1999)
  9. Pardo-Yissar V, Gabai R, Shipway AN, Bourenko T, Willner I, Adv. Mater., 13(17), 1320 (2001)
  10. Boal AK, Rotello VM, J. Am. Chem. Soc., 124(18), 5019 (2002)
  11. Boal AK, Rotello VM, J. Am. Chem. Soc., 122(4), 734 (2000)
  12. Oh SD, Byun BS Lee SH, Choi SH, Macromol. Res., 14(2), 194 (2006)
  13. Oh SD, Byun BS, Lee S, Choi SH, Kim MI, Park HG, Macromol. Res., 15(4), 285 (2007)
  14. Lin Z, Gilbert B, Liu QL, Ren GQ, Huang F, J. Am. Chem. Soc., 128(18), 6126 (2006)
  15. Schmid G, Morun B, Malm JO, Angew. Chem.-Int. Edit., 28, 778 (1989)
  16. Manorama SV, Reddy KM, Reddy CVG, Narayanan S, Paja PR, Chatterji PR, J. Phys. Chem. Solids, 63, 135 (2002)
  17. Zhou Y, Itoh H, Uemura T, Naka K, Chujo Y, Langmuir, 18(13), 5287 (2002)
  18. Park C, Rhue M, Lim J, Kim C, Macromol. Res., 15(1), 39 (2007)
  19. Klabunde KJ, Habdas J, Cardenas-Trivino G, Chem. Mater., 1, 481 (1989)
  20. Elshall MS, Slack W, Macromolecules, 28(24), 8456 (1995)
  21. Quaroni L, Chumanov G, J. Am. Chem. Soc., 121(45), 10642 (1999)
  22. Johans C, Clohessy J, Fantini S, Kontturi K, Cunnane VJ, Electrochem. Commun., 4, 227 (2002)
  23. Sarma TK, Chowdhury D, Paul A, Chattopadhyay A, Chem. Commun., 1048 (2002)
  24. Nicolais L, Carotenuto G, Metal-polymer nanocomposites, Wiley, New Jersey (2005)
  25. Cha DI, Kim KW, Chu GH, Kim HY, Lee KH, Bhattarai N, Macromol. Res., 14(3), 331 (2006)
  26. Park K, Jung HJ, Kim JJ, Ahn KD, Han DK, Ju YM, Macromol. Res., 14(5), 552 (2006)
  27. Jung YH, Kim HY, Lee DR, Park SY, Khil MS, Macromol. Res., 13(5), 385 (2005)
  28. Auang ZM, Zhang YZ, Kotaki M, Ramakrishna S, Compos. Sci. Technol., 63, 2223 (2003)
  29. Son WK, Youk JH, Lee TS, Park WH, Macromol. Rapid Commun., 25(18), 1632 (2004)
  30. Park H, Lee KY, Lee SJ, Park KE, Park WH, Macromol. Res., 15(3), 238 (2007)
  31. Feng QL, Wu J, Chen GQ, Cui FZ, Kim TN, Kim JO, J. Biomed. Mater. Res., 52, 662 (2000)
  32. Kim GM, Wutzler A, Radusch HJ, Michler GH, Simon P, Sperling RA, Parak WJ, Chem. Mater., 17, 4949 (2005)
  33. Bai J, Li Y, Yang S, Du J, Wang S, Zheng J, Wang Y, Yang Q, Chen X, Jing X, Solid State Commun., 141, 292 (2007)
  34. Wang YZ, Li YX, Sun G, Zhang GL, Liu H, Du JS, Yang SA, Bai J, Yang QB, J. Appl. Polym. Sci., 105(6), 3618 (2007)
  35. Brust M, Walker M, Bethell D, Schiffrin DJ, Whyman R, J. Chem. Soc., Chem. Commun., 801 (1994)
  36. Son WK, Youk JH, Lee TS, Park WH, Polymer, 45(9), 2959 (2004)
  37. Balan L, Burget D, Eur. Polym. J., 42, 3180 (2006)