The problem of mixing fuel and air is the essential point of low emission combustion in gas turbines. In premixed combustors and fuel staged combustors the quality of the fuel-air mixture is the determinant parameter for the amount of emissions of nitric oxides (NOx). The nearly perfect preparation of the fuel-air mixture is also a condition for trouble-free operation in catalytical combustion. Prevaporization of liquid fuels hampers the process of mixing. So the investigative work at the Department of Steam and Gas Turbines at the University of Bochum concentrated on experiments with liquid fuels. The results show that there is a great potential of reducing NOx emission even with liquid fuels and reveal the key role of prevaporization and mixing. The experiments were carried out at a premix combustion test rig at moderate pressure. By using the technique of planar-laser induced fluorescence (LIF), highly time and spatially resolved measurements of fuel concentrations were yielded from the experiments. The optical measurements showed the structure of the mixture held of fuel and air in the zone downstream of the flameholder. The pollutant emissions were simultaneously monitored with conventional gas analysers. As the main result, the strong dependence of the pollutant emissions on the mixture could be clearly revealed. On one hand the homogeneity over the cross-section of the combustor was the main condition for low emission combustion. On the other hand the time-resolved two-dimensional LIF images of the turbulent mixture field showed that the instationary distribution also had a considerable influence on the rate of emissions. Even the mixture of static mixers contained spatial and temporal inhomogeneities, which could be observed by using the LIE-technique but not with conventional methods.