Synthesis and surface characterization of silica nanoparticles from industrial resin waste controlled by optimal gelation conditions

Tzong-Horng Liou; Huan-Siang Lin

Journal of Industrial and Engineering Chemistry, Vol.18, No.4, 1428-1437, July, 2012

DOI10.1016/j.jiec.2012.02.001 Export Citation

Synthesis and surface characterization of silica nanoparticles from industrial resin waste controlled by optimal gelation conditions

Tzong-Horng Liou^†, and Huan-Siang Lin

Department of Chemical Engineering, Ming Chi University of Technology, 84 Gungjuan Rd., Taishan, New Taipei 24301, Taiwan

E-mail:

Electrical and electronic waste is one of the fastest-growing industrial wastes. This paper examined the silicon extracted form electronic packaging resin ash with a subsequent acidic treatment for silica nanoparticle production. The experimental results showed that sample surface characteristics were highly dependent on the sodium silicate concentration, aging temperature, aging time, gelation pH, etc. The surface areas of the silica ranged from 214 to 664 m2/g and the particle sizes ranged from 5 to 30 nm. The results of this study will provide a sensible solution for the recycling of silicon-containing industrial waste for a new value-added product.

Keywords:Electronic packaging resin;Silica;Nanoparticle;Mesoporous;Recycling

[References]

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Brunauer S, Emmett PH, Teller E, J. Am. Chem. Soc., 60, 309 (1938)
Liou TH, Chem. Eng. J., 158(2), 129 (2010)
Kalapathy U, Proctor A, Shultz J, Bioresour. Technol., 85(3), 285 (2002)
Yun CH, Park YH, Oh GH, Park CR, Carbon., 41, 2009 (2003)
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Liou TH, Carbon., 42, 785 (2004)
Katcho NA, Urones-Garrote E, A´ vila-Brande D, Go´ mez-Herrero A, Urbonaite S, Csillag S, Lomba E, Agullo´ -Rueda F, Landa-Ca´ novas AR, Otero-Dı´az LC, Chem.Mater., 19, 2304 (2007)
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Liou TH, Wu SJ, J. Hazard. Mater., 171(1-3), 693 (2009)
Kalapathy U, Proctor A, Shultz J, J. Chem. Technol. Biotechnol., 75(6), 464 (2000)
Silverstein RM, Webster FX, Kiemle DJ, Spectrometric Identification of Organic Compounds, 7th ed., John Wiley & Sons, Inc, USA (2005)
Liou TH, Mater. Sci. Eng. A . Struct., 364, 313 (2004)
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[Referenced By]

[1] Kim HJ, Han B, Kim YJ, Yoa SJ, J. Aerosol Sci., 41, 987 (2010)

[2] Chen D, Bi X, Liu M, Huang B, Sheng G, Fu J, Chemosphere., 82, 1246 (2011)

[3] Shih LH, Resour. Conserv. Recycl., 32, 55 (2001)

[4] Sun YY, Zhang ZQ, Wong CP, Polymer, 46(7), 2297 (2005)

[5] Liou TH, J. Hazard. Mater., 103(1-2), 107 (2003)

[6] Giaquinto A, Liu Z, Bach A, Kazakevich Y, Anal. Chem., 80, 6358 (2008)

[7] Vakarelski IU, Brown SC, Basim GB, Rabinovich YI, Moudgil BM, ACS Appl.Mater. Interfaces., 2, 1228 (2010)

[8] Morpurgo M, Teoli D, Pignatto M, Attrezzi M, Spadaro F , Realdon N, Acta Biomater., 6, 2246 (2010)

[9] Jouault N, Vallat P, Dalmas F, Said S, Jestin J, Boue F, Macromolecules, 42(6), 2031 (2009)

[10] Brinker CJ, Scherer GW, Sol-Gel Science, the Physics and Chemistry of Sol-Gel Processing, Academic Press, Inc., San Diego, CA (1990)

[11] Liou TH, Chem. Eng. J., 98(1-2), 39 (2004)

[12] Valdes-Solis T, Marban G, Fuertes AB, Catal. Today, 116(3), 354 (2006)

[13] Ha JW, Do YW, Park JH, Han CH, J. Ind. Eng. Chem., 15(5), 670 (2009)

[14] Goodman AL, Energy Fuels, 23(1), 1101 (2009)

[15] Huang Z, Cui F, Kang H, Chen J, Zhang X, Xia C, Chem. Mater., 20, 5090 (2008)

[16] Kim J, Wainaina J, Na JS, J. Ind. Eng. Chem., 17(4), 681 (2011)

[17] Isobe H, Utsumi S, Yamamoto K, Kanoh H, Kaneko K, Langmuir, 21(17), 8042 (2005)

[18] Tang Q, Wang T, J. Supercrit. Fluids, 35(1), 91 (2005)

[19] Bai GH, Teng W, Wang XG, Zhang H, Xu P, Fuel Process. Technol., 91(2), 175 (2010)

[20] Karami A, J. Colloid Interface Sci., 331(2), 379 (2009)

[21] Hartono SB, Qiao SZ, Jack K, Ladewig BP, Hao ZP, Lu GQ, Langmuir, 25(11), 6413 (2009)

[22] Dhokte AO, Khillare SL, Lande MK, Arbad BR, J. Ind. Eng. Chem., 17(4), 742 (2011)

[23] Liou TH, Chem. Eng. J., 171(3), 1458 (2011)

[24] Brunauer S, Emmett PH, Teller E, J. Am. Chem. Soc., 60, 309 (1938)

[25] Liou TH, Chem. Eng. J., 158(2), 129 (2010)

[26] Kalapathy U, Proctor A, Shultz J, Bioresour. Technol., 85(3), 285 (2002)

[27] Yun CH, Park YH, Oh GH, Park CR, Carbon., 41, 2009 (2003)

[28] Hessien MM, Rashad MM, Zaky RR, Abdel-Aal EA, El-Barawy KA, Mater. Sci.Eng. B . Solid., 162, 14 (2009)

[29] Tsai MS, Mater. Sci. Eng. B . Solid., 106, 52 (2004)

[30] Affandi S, Setyawan H, Winardi S, Purwanto A, Balgis R, Adv. Powder Technol., 20(5), 468 (2009)

[31] Schlomach J, Kind M, J. Colloid Interface Sci., 277(2), 316 (2004)

[32] Munozaguado MJ, Gregorkiewitz M, J. Colloid Interface Sci., 185(2), 459 (1997)

[33] Gregg SJ, Sing KSW, Adsorption, Surface Area and Porosity, 2nd ed., Academic Press, London (1982)

[34] Liou TH, Carbon., 42, 785 (2004)

[35] Katcho NA, Urones-Garrote E, A´ vila-Brande D, Go´ mez-Herrero A, Urbonaite S, Csillag S, Lomba E, Agullo´ -Rueda F, Landa-Ca´ novas AR, Otero-Dı´az LC, Chem.Mater., 19, 2304 (2007)

[36] Chandrasekar G, You KS, Ahn JW, Ahn WS, Micropor. Mesopor. Mater., 111, 455 (2008)

[37] Yao YQ, Ying YF, Luo MF, Wang YJ, Ma JM, Mater. Lett., 61, 192 (2007)

[38] Liou TH, Wu SJ, J. Hazard. Mater., 171(1-3), 693 (2009)

[39] Kalapathy U, Proctor A, Shultz J, J. Chem. Technol. Biotechnol., 75(6), 464 (2000)

[40] Silverstein RM, Webster FX, Kiemle DJ, Spectrometric Identification of Organic Compounds, 7th ed., John Wiley & Sons, Inc, USA (2005)

[41] Liou TH, Mater. Sci. Eng. A . Struct., 364, 313 (2004)

[42] Witoon T, Chareonpanich M, Limtrakul J, Mater. Lett., 62, 1476 (2008)