화학공학소재연구정보센터
학회 한국화학공학회
학술대회 2018년 가을 (10/24 ~ 10/26, 대구 EXCO)
권호 24권 2호, p.2076
발표분야 촉매 및 반응공학(Catalysis and Reaction Engineering)
제목 Modification of NiTiO3 visible light photocatalysts using Nb compounds
초록 Herein we prepared two types of Niobium-containing photocatalysts, Nb-doped NiTiO3 and Nb2O5/NiTiO3 heterojunction. Nb-doped NiTiO3 was synthesized via modified Pechini method followed by a solvothermal treatment and calcination. Nb2O5/NiTiO3 heterojunctions was synthesized by a hydrolysis-loading method. The structural and optical properties were characterized by XRD, Raman, FT-IR, SEM, TEM, XPS, N2 adsorption/desorption technique, UV–vis spectra and PL spectra. Nb-containing photocatalysts were also examined in the degradation of methylene blue (MB) under visible light irritation to understand the influence of the Nb doping into the lattice structure or Nb2O5 heterojunction structure on the photocatalytic behavior. In the results Nb-doped NiTiO3 exhibited higher photocatalytic activity than pure NiTiO3 while Nb2O5 heterojunction with NiTiO3 caused a decrease in photocatalytic activity.
저자 정해원1, 장개명1, Pham Thanh Truc1, Yong Men2, 신은우1
소속 1울산대, 2Shanghai Univ. of Engineering Science
키워드 촉매 및 반응공학
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