화학공학소재연구정보센터
학회 한국재료학회
학술대회 2007년 가을 (11/02 ~ 11/02, 성균관대학교)
권호 13권 2호
발표분야 나노생체재료
제목 Sol-Gel법에 의한 calcium titanate buffer layer processe와 Hydroxyapatite 코팅
초록 The present study evaluates this effect of a (CaTiO3: CTO) intermediate coating on the bonding strength of HA to Ti6Al4V (TAV) substrate. The CTO and HA precursors were coated on TAV by sol–gel dip-coating method. A single CTO layer (~ 500 nm thickness) was coated and heat treated at 750°C prior to five times of HA coating. The HA coating showed a thickness of 8–10 μm, after the heat treatment at 600 °C. Phase formation, surface morphology, and interfacial microstructure were investigated by x-ray diffraction (XRD) and scanning electron microscopy (SEM). SEM observations revealed no cracks on the HA/CTO surface. However surface cracks were observed when HA was directly coated on TAV. The bonding strength of HA/CTO increased almost three times compare to direct HA coatings. The higher bonding strength on CTO coated sample could be attributed to the formation of micro-cracks, the high surface roughness and high interfacial bonding between HA and CTO layer.
저자 이병천1, A. Balakrishnan1, 김택남1, 박중근2
소속 1배재대, 2한국과학기술원 재료공학과
키워드 Sol-gel; Surface cracks; Hydroxyapatite; Bonding strength
E-Mail