| 학회 | 한국공업화학회 |
| 학술대회 | 2020년 가을 (10/28 ~ 10/30, 광주 김대중컨벤션센터(Kimdaejung Convention Center)) |
| 권호 | 24권 1호 |
| 발표분야 | 포스터-콜로이드·계면화학 |
| 제목 | Study of Lattice Parameter of Cladding Materials using In-Situ High-Temperature X-ray Diffraction. |
| 초록 | Crystal structural properties of cladding materials in the temperature range of 30℃~1430℃ were measured using in-situ high-temperature X-ray diffraction (HT-XRD). The powder diffraction pattern of the Hexagonal crystal structure of Zr metal observed at 30℃ started to vanish above 1110℃ for Zr and 1230℃ for Zr alloy owing to oxidation, resulting in a composition with monoclinic ZrO2, tetragonal ZrO2, and rhombohedral Zr3O. Furthermore, cell parameter calculation using Pawley refinement method of in situ HT-XRD patterns, we demonstrated that the lattice thermal expansion in cladding materials occurred in a stable manner compared to that in Zr, which contribute to the enhancement of its mechanical properties via thermal treatment. |
| 저자 | 이동우1, 윤영상2, 박정미1, 임상호1 |
| 소속 | 1한국원자력(연), 2영남대 |
| 키워드 | Zirconium; Cladding; Ht-XRD; Lattice parameter |
