| 학회 |
한국공업화학회 |
| 학술대회 |
2004년 가을 (10/29 ~ 10/30, 호서대학교(아산캠퍼스)) |
| 권호 |
8권 2호 |
| 발표분야 |
계면화학 |
| 제목 |
Synthesis of hydrophobic MCM-41 |
| 초록 |
The pure silica MCM-41 molecular sieve was synthesized with tetraethyl orthosilicate (TEOS) as the source of silica, and cetyltrimethylammonium bromide (CTAB) as a template under hydrothermal condition. Several synthesis parameters such as temperature, the ratio of Si and surfactant, aging time and pH adjustment of the mixture were investigated for the optimum preparation process. The hydrophobic MCM-41 was obtained by introducing trimethylsilyl to MCM-41 by refluxing the mixtures of trimethylsilyl chloride ((CH3)3SiCl) and hexamethyldisiloxane (((CH3)3Si)2O) with MCM-41 for overnight under N2. The dried products were comparatively characterized using XRD, TEM and adsorption isotherms of nitrogen. |
| 저자 |
Yan Jia1, 김동표1, Anjie Wang2
|
| 소속 |
1충남대, 2Dalian Univ. of Technology |
| 키워드 |
hydrophobic MCM-41 |
| E-Mail |
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