화학공학소재연구정보센터
학회 한국공업화학회
학술대회 2015년 가을 (11/04 ~ 11/06, 제주국제컨벤션센터(ICCJEJU))
권호 19권 2호
발표분야 무기재료_포스터
제목 A facile synthesis of mesoporous composite materials by a particle coagulation-precipitation method
초록 Mesoporous composite materials of one dimensional particles and two-dimensional nano-sheets have been prepared successfully by a simple coagulation-precipitation method. Ferromagnetic magnetite, spinel-type crystalline copper chromite, and amorphous copper manganate was used as one dimensional particles. While the synthetic hectorite particle was used as two-dimensional nano-sheet. In a typical process metal oxide particles were thoroughly dispersed in aqueous solution and then the pre-swelled silicate dispersion was added to the particle suspension under vigorous stirring, followed by adjusting the pH of mixed suspension to 2~3 using acetic acid, resulted in a highly viscous gel-like product. The gel-like product was precipitated by centrifuging, washed with the mixed solvent of distilled water and acetone, then dried at 120℃ for 2h. Thus prepared composite powders exhibited dramatically enhanced specific surface area and pore volume.
저자 한양수1, 황지연2, 이지호1
소속 1(주)세일에프에이 기업부설(연), 2(주)나노스페이스 나노물질(연)
키워드 mesoporous; layer silicate; acidic; nanoparticle
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