화학공학소재연구정보센터
학회 한국고분자학회
학술대회 2010년 가을 (10/07 ~ 10/08, 대구 EXCO)
권호 35권 2호
발표분야 고분자 구조 및 물성
제목 Preparation and characterization of high aspect ratio nanofibers in polyamide-6 by using electrospinning
초록 we report on the high aspect ratio polyamide-6 nanofibers prepared by using electrospinning technique. The morphological, structural characterizations and thermal properties of the polyamide-6 nanofibers were determined using field-emission scanning electron microscopy (FE-SEM), X-ray diffraction (XRD), thermogravimetry (TGA), Raman spectroscopy, Fourier transform-infrared (FT-IR) spectroscopy and transmission electron microscopy (TEM). In order to accurately characterize the high aspect ratio nanofiber structure by the direct identification of mass resolved chains, we performed matrix-assisted laser desorption ionization time-of-flight (MALDI-TOF). FE-SEM images revealed that high aspect ratio polyamide-6 nanofibers bound between the main fibers. The diameter of the polyamide-6 nanofibers were observed to be in the range of 75 to 110 nm, whereas the high aspect ratio structures consisted of regularly distributed very fine nanofibers with diameters of about 9 to 28 nm.
저자 니말라, 남기택, 백우일, R. Navamathavan, 김학용
소속 전북대
키워드 eletrospinning; polyamide-6; high aspect ratio
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