| 학회 |
한국화학공학회 |
| 학술대회 |
2019년 봄 (04/24 ~ 04/26, 제주국제컨벤션센터) |
| 권호 |
25권 1호, p.835 |
| 발표분야 |
재료(Materials) |
| 제목 |
Synthesis of UiO-66 using microwave-assisted continuous reactor and its application for VOC recovery |
| 초록 |
UiO-66 has been widely used for many applications due to its high surface area, and excellent chemical and thermal stability. Conventionally, UiO-66 has been prepared in autoclave by solvothermal synthesis, which requires a lengthy reaction time producing small amount of product. In this work, multi-grams of UiO-66 was repidly produced in a continuous tubular reactor under microwave irradiation. The metal salt and organic linker precursor solutions were continuously introduced into the tubular reactor by a microfluidic syringe pump system. The results showed that UiO-66 with high yield, porosity and crystallinity was produced within a short reaction time of 10 min. The characteristics of UiO-66 was affected by reaction temperature, residence time, and modulator concentration. The UiO-66 was tested for toluene adsorption at various adsorption temperatures. |
| 저자 |
김진수1, The Ky Vo1, 유계상2, 송무근2, 김대근2, Le Van Nhieu1
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| 소속 |
1경희대, 2서울과학기술대 |
| 키워드 |
재료 |
| E-Mail |
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| 원문파일 |
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