| 학회 |
한국공업화학회 |
| 학술대회 |
2015년 봄 (04/29 ~ 05/01, BEXCO (부산)) |
| 권호 |
19권 1호 |
| 발표분야 |
정밀화학_포스터 |
| 제목 |
Silicon nitride (SiN) coating optimization on carbon fiber surfaces by wet-thermal methods |
| 초록 |
In this work, the silicon nitride on carbon fiber surfaces were synthesized directly from the wet-thermal reaction via an 3-aminopropyltriethoxysilane (APS) without additives under N2/NH3 mix gas at high temperature (1400℃). Silicon nitride synthesis was investigated in terms of heating temperature, time, and content of APS. It was found that most combined silanol group (Si-OH) in carbon fiber surfaces has changed to silicon nitride at 1400℃ in an atmosphere of N2/NH3 mix gas during thermal treatment steps of silane-treated carbon fibers. As a result, the morphology of the resulting silicon nitride appeared as a whisker shape. Synthesis of silicon nitride was conjectured that the transformation occurs via the gas phase and is affected by reaction time. |
| 저자 |
김현혜1, 한웅2, 이해성3, 김병주2
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| 소속 |
1한국탄소융합기술원 / 전주대, 2한국탄소융합기술원, 3전주대 |
| 키워드 |
silicon nitride (SiN); silane coupling agent; synthesis; reaction time; NH3/N2 mix gas
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| E-Mail |
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