초록 |
Co–Ni double hydroxides were directly deposited onto Ni foam by the potentiostatic deposition method at −0.75 V vs. SCE using different molar ratios of Co(NO3)2•6H2O and Ni(NO3)2•6H2O in distilled water without adding any surfactant and conducting agent. Structural and morphological studies were done by using X-ray diffraction analysis, Energy dispersive X-ray spectroscopy, Scanning electron microscopy and Transmission electron microscopy. A network of CoxNi1−x double hydroxide nanosheets was obtained. X-ray photoelectron spectroscopy was used to study the oxidation states of Co and Ni. Electrodeposited Co–Ni layered double hydroxides were studied for methanol oxidation application. This work was supported by Basic Science Research Program through the National Research Foundation of Korea (NRF) funded by the Ministry of Education (NRF 2016R1D1A1B03930855). |