화학공학소재연구정보센터
학회 한국공업화학회
학술대회 2012년 봄 (05/09 ~ 05/11, 김대중컨벤션센터)
권호 16권 1호
발표분야 화학공정
제목 Isolation of toxic aqueous essential oil from Chamaecyparis obtusa using LLE and SPE
초록 An extraction method for the removal of five toxic aqueous essential oils (α-terpinene, γ-terpinene, linalool, α-terpineol, and α-terpinyl acetate) in Chamaecyparis obtusa (C. obtusa) by liquid-liquid extraction (LLE) and solid-phase extraction (SPE) combined with gas chromatography. The best LLE conditions were as follows: extraction solvent, 1-octanol, and an essential oil:1-octanol ratio of 7:3. The best SPE conditions were as follows: sorbent, C18; and washing and elution step solvents of 2 mL 1-octanol and 1 mL water, respectively. Under these conditions, of the five toxic aqueous compounds α-terpinene, γ-terpinene and linalool were not detected, and only small amounts of α-terpineol (6.75 ng/g) and α-terpinyl acetate (2.77 ng/g) were detected. GC-FID was used to detect the five toxic aqueous essential oils.
저자 이유리1, 김은철2, 노경호3
소속 1인하대, 2College of Food Science & Technology, 3Shanghai Ocean Univ.
키워드 Liquid-liquid extraction; Solid-phase extraction; Toxic aqueous; Essential oils
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