화학공학소재연구정보센터
학회 한국공업화학회
학술대회 2005년 가을 (10/28 ~ 10/29, 건국대학교)
권호 9권 2호
발표분야 무기재료
제목 Preparation of Spherical SiO2 Nanoparticles from Sprayed Droplets of Tetraethylorthosilicate by the Flame Spray Pyrolysis
초록 Amorphous spherical silica (SiO2) nanoparticles from 12 to 47nm in average particle diameter were synthesized from sprayed droplets of TEOS by the flame spray pyrolysis. TEOS concentration, maximum flame temperature, and residence time of reactants in the flame were chosen as key experimental variables. As the TEOS concentration in the flame increased, the average particle diameter of the SiO2 nanoparticles having narrow size distribution increased. Larger SiO2 nanoparticles were synthesized as hydrogen and oxygen flow rate decreased in the flame, respectively. Average particle diameter decreased as the residence time of the precursor increased by controlling of carrier gas flow rate.
저자 장희동, 장한권
소속 한국지질자원(연)
키워드 synthesis; SiO2; flame spray pyrolysis
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