화학공학소재연구정보센터
학회 한국화학공학회
학술대회 2006년 봄 (04/20 ~ 04/21, 대구 인터불고 호텔)
권호 12권 1호, p.998
발표분야 재료
제목 Shape-Controlled Synthesis of Flower-like ZnO Nanostructures via Simple Solution Chemistry
초록 Flowers-shaped ZnO nanostructures have been successfully synthesized by reaction of aqueous solution of zinc nitrate and NaOH at low temperature (90 °C). To examine the morphology and growth process of ZnO nanostructures, time dependent (7, 9 and 11 hrs) experiments were carried out without changing other reaction parameters. Scanning electron microscopy images revealed that the reaction carried out for 7 hrs resulted in formation of ZnO flowers with triangular- shaped leaves and some irregular nanoparticles of ZnO desiminated around flowers. When the reaction time is increased upto 9 hrs ZnO flower in clusters are obtained. Further increasing the reaction time to 11 hrs resulted in monodispersed-flower shaped ZnO nanostructures. XRD and TEM analysis revealed that obtained flower shaped nanostructures are single crystalline with wurtzite hexagonal phase. Finally, growth mechanisms for the formation of these ZnO nanostructures were discussed based on the obtained results.
저자 Ahsanulhaq, 김상훈, 라현욱, 한윤봉
소속 전북대
키워드 Shape-Controlled Synthesis; Flower-like ZnO Nanostructures
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