학회 | 한국화학공학회 |
학술대회 | 2012년 가을 (10/24 ~ 10/26, 부산 BEXCO) |
권호 | 18권 2호, p.2261 |
발표분야 | 재료 |
제목 | Study on optical properties of copper sulfide nanoparticles synthesized by a solvothermal method |
초록 | In the study, copper sulfide (CuxS) nanoparticles, electric conductors, have been synthesized by a solvothermal reaction of copper sulfate pentahydrate (CuSO4·5H2O) and sodium sulfide pentagydrate (Na2S·5H2O) in aqueous solutions. The molar ratio of Cu/S was controlled by parameters such as reaction time, temperature, and pH since that affected optical properties of copper sulfide. The reaction temperature was optimized at 95℃ through the experiments from room temperature to near 100℃. The effects of pH and reaction time were performed from 2 to 13 and from 0.5 h to 2 h, respectively. The samples are conducted optical properties by X-ray diffraction (XRD), emission scanning electron microscopy (FESEM), energy dispersive X-ray spectrometer (EDS), and UV-visible spectrometer. The nanoparticles obtained from the study can be applied for the window film with a high light transmittance and UV-cutting. |
저자 | 이상은, 정동혁, 김문선, 김병우 |
소속 | 성균관대 |
키워드 | Copper sulfide; Nanoparticles; Solvothermal method |
원문파일 | 초록 보기 |