화학공학소재연구정보센터
학회 한국고분자학회
학술대회 2006년 봄 (04/06 ~ 04/07, 일산킨텍스)
권호 31권 1호
발표분야 기능성 고분자
제목 A Study on Preparation of Carbon Aerogels by a Sol-gel Polymerization
초록 Carbon aerogels are novel mesoporous carbon materials with many interesting properties, such as low mass densities, continous pore structures, high surface areas, great mesopore volume and high electrical conductivity. Carbon aerogel was prepared by a sol-gel polymerization of resorcinol with formaldehyde, and sodium carbonate was added as a catalyst. Physical properties of carbon areogel were characterized by infrared spectroscopy (IR), X-ray diffraction (XRD), and scanning electron microscopy (SEM). It is found that carbon aerogel is amorphous materials with a pearly network structure, and it consists of one or two diffuse X-ray peaks. With the addition of sodium carbonate, an CO2 supercritical drying technique was developed for the fabrication of carbon arogels. As a result, the addition of sodium carbonate increases the size of carbon nanoparticles and the pore size of the aerogels.
저자 이은정1, 권수한2, 박수진1
소속 1한국화학(연), 2충북대
키워드 carbon aerogel; sol-gel polymerization; supercritical drying
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