화학공학소재연구정보센터
학회 한국화학공학회
학술대회 2008년 가을 (10/23 ~ 10/24, 부산 BEXCO)
권호 14권 2호, p.3438
발표분야 재료
제목 Aging effects on hexagonal pencil like zinc oxide nanostructures
초록 zinc oxide nanorods (Pencil like) were synthesized by solution methods in presence of zinc acetate dihydrate (Zn(Ac)2.2H2O) and alkali sodium hydroxide (NaOH) at 75°C for the different ageing time (12, 24, 36,48 and 60 hours) intervals. The morphological observation was carried out by the field emission scanning electron microscopy (FESEM). It reveals that as the (refluxing) time increases the size (length and diameter) of zinc oxide nanorods is increases. Further, the morphological characterization was also carried out by using transmission electron microscopy (TEM), selected area electron diffraction (SAED) pattern and high-resolution transmission electron microscopy (HRTEM). TEM image is closely consistent with the FESEM observations. The crystallinity of the product was observed by the X-ray diffraction pattern. The optical property of the hexagonal zinc oxide nanorods was characterized by the using UV-vis spectrophotometer. A strong peak of zinc oxide was observed at 373 nm which is the characteristic peak of zinc oxide.
저자 송민우, Rizwan Wahab, S. G. Ansari, 김영순, 이경섭, 신형식
소속 전북대
키워드 Aging; ZnO; Solution method
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