화학공학소재연구정보센터
학회 한국화학공학회
학술대회 2015년 가을 (10/21 ~ 10/23, 일산 KINTEX)
권호 21권 2호, p.2118
발표분야 재료
제목 In situ analysis of the crystallization separation using nano porous gravimetric electrode
초록 Sensors that can covert various environmental information such as physical, chemical, and biological information to human-perceptible data have widened applications, and the demand for the sensors tend to be increased in these days.  More effective methods are also proposed by the development of nano-technology. In this study, a quartz crystal was used as a device for analyzing the microscopic mass change. Nano-reactor on an analyzing chip (NAC) has a porous structure on the electrode surface, and it can provide a high reproducibility, reliability and functionality. NAC quartz crystal was utilized in crystallization analysis of GS-host molecules. The fabrication of NAC quartz crystal was performed following the undescribed procedure. PSB solution sprayed on the commercial quartz crystal to create a monolayer, then the elctrodeposition was applied to the crystal at the constant voltage of -0.7 V(vs. SCE) in  gold(lll) chloride soulution. The surface of the  crystal was modified with aminopropyltriethoxysilane using self-assembly procedure. Molecular recognition and crystallization experiments were performed using GS-host molecures, G2BPDS and G2NDS as well as target molecules.  In this study, we confirmed the excellent functionality of NAC quartz crystal for monitoring the crystallization behaviour between GS-host molecules and target molecules.
저자 김종민, 장상목, 김용우, 이요한
소속 동아대
키워드 NAC quartz crystal; Electrodeposition
E-Mail
원문파일 초록 보기